GCMS quantitation report, sample AE11933, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report • Data File : C:\MSDCHEM\1\DATA\0610022\11933 .D Vial: 10 Acq On : 10 Jun 2002 6:21 pm Operator: Sample : gc/ms scan 6/7 fb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 5 Borane, trifluoro­ Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 3.83 0.98 ug/L 812169 1,4-dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Borane, trifluoro- 68 BF3 007637-07-2 2 2 2-Chloroethanol 80 C2H5C1O 000107-07-3 2 3 Boron trifluoride etherate 142 C4H10BF3O 000109-63-7 2 4 2-Chloroethanol 80 C2H5C1O 000107-07/3 2 Abundance Scan 128 (3.831 min): 11933.D (-126) (-) m/z 49.10 100.00% 49

5000 84 36 3.40 3.60 3.80 4.00 4.20 ....................... ..... ----- m/z 48.10 34.79% 1/* 0- ■'' । ■ ■ ■ ■ । ■ ■ ■ • । ■ ■ ■ ■ । ■ • m/z-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #12321: Borane, trifluoro- 49

5000 i ' ‘ ' i ■ ■ ' ■ i ■ ‘ ■ i ■ ■ 3.40 3.60 3.80 4.00 4.20 m/ z 84.00 27.84% 68 0- 11 ■ 19 .30 38 .. ■ i.... ।... 11 . । i. miz-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #108328:2-Chloroethanol 31

3.40 3.60 3.80 4.00 4.20 5000 m/z 84.95 23.45% 44

0- ‘ * i * ‘ ‘ ' i ■ ‘ ‘ ‘ i .37,-1.151,57,63. 80 ■ i ■ ‘ ‘ "[ ।। ।. m/z-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #1099: Boron trifluoride etherate T 1 1 1 1 1 ' 1 1 1 1 1 1 ' 1 I ' ' 31 3.40 3.60 3.80 4.00 4.20 m/z 51.10 22.04% 59 5000 45 74

0 ■ ■ i ■ 15425 1' 39,1,1, ■, , 1 66 ,81 93 127 n/z-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 3.40 3.60 3.80 4.00 4.20

11933.D 060302.M Tue Jun 11 08:23:07 2002 Page 8

NYC-WTC_000015729