GCMS quantitation report, sample AE11933, June 2002

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' Data File : C:\MSDCHEM\1\DATA\0610022\11933.D Vial: 10 Acq On : 10 Jun 2002 6:21 pm Operator: Sample : gc/ms scan 6/7 fb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 4 1,3-Dioxol-2-one Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

3.81 0.50 ug/L 415548 1,4-dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,3-Dioxol-2-one 86 C3H203 000872-36-6 4/ 2 1,3-Dioxol-2-one 86 C3H203 000872-36-6 4 3 Phosphonic difluoride 86 F2HOP 014939-34-5 4 4 Imidazol, 4-fluoro- 86 C3H3FN2 030086-17-0 4 Abundance Scan 124 (3.808 min): 11933.D (-123) (-) m/z 86.00 100.00% 83

49 5000

36 3.40 3.60 3.80 4.00 4.20 Of lr Mayunu I ■ ■ ■ ■ i ‘ ■ ■ ■ i ■ ■ ■ ■ i ■ • ■ ■ i''1 • i" ■ ■ i •' ■ m/z 84.. 00 68.55% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #116747: 1,3-Dioxol-2-one 29 83

42 5000 3.40 3.60 3.80 4.00 4.20 58 m/z 49.10 57.72% 01 — ———————— 2326 32.36391.45.50.55.11.663 67 71 77 83 89— ‘‘l‘‘‘‘1‘4‘*1****1****i miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #34604:1,3-Dioxol-2-one 83 29 3.40 3.60 3.80 4.00 4.20 42 m/z 36.10 12.40% 5000

nfe-> 17 14

26 0 TTTTTTTTTT+ TTTTTH 32,38 1,4548,53, 64 71 58

■ I * j । । ■ l •i>1 1>• l * * < >l • * * * I 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 89—7 AWootp/Hnaw- Abundance #34889: Phosphonic difluoride ’41***+11*’*1+’’’I’1 85 3.40 3.60 3.80 4.00 4.20 m/z 35.10 5.98% 5000 69 WWA, Jw/ "Apkop 66 47 50 0 ••i‘ 31 > j •" • i • * ■ ■ i" • • i ‘ " i1 ■ * * i “ ‘ * I" " 11 mP i ■" ■ i “ i ■ ■ " i ■ ■ ■ ■ i" n/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.40 3.60 3.80 4.00 4.20

11933.D 060302.M Tue Jun 11 08:23:04 2002 Page 7

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