GCMS analysis results for sample AE12162, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C: \MSDCHEM\1\DATA\052302\12162.D Vial: 15 Acq On : 23 May 2002 9:22 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C: \MSDCHEM\1\METHODS\052202 .M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 7 1,3-Dioxol-2-one Concentration Rank 4

R.T. EStCone Area Relative to ISTD R.T.

3.94 1.27 ug/L 776362 1,4 -Dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3-Dioxol-2-one 86 C3H203 000872-36-6 5 2 1,3-Dioxol-2-one 86 C3H203 000872-36-6 5 3 Formamide, N-(cyanomethyl)- 84 C3H4N2O 005018-27-9 5 4 Ethenamine, N-methyl-N-nitroso- 86 C3H6N20 004549-40-0 3 Abundance Scan 147 (3.943 min): 12162.D (-145) (-) m/z 86.00 100.00% 85

5000 51

43 82 36 48 3.60 3.80 4.00 4.20

niz-> —444+ O+ ‘ I‘*‘‘A-++‘IIA‘*Z‘‘‘*I‘**+H+ 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ■ i “ ■ ‘ i ■ “' i ■ “ • i “ “ i i “■ ’ ’1144+1’4* m/z .84.00 45.52% Abundance #116748:1,3-Dioxol-2-one 85 29 42 5000 ' ■ i ' ‘ ' i 1 ' ■ ■ i 1 ■ ■ ‘ i ■ ■ ‘ ■ i 1 3.60 3.80 4.00 4.20 58 m/z/ 51.10 44.65% 26 l 11548 55 62 74 83 Ot 11 H TTTTTTTPTOTHI -I t- J • i J > i1 niz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 95 Abundance #34604:1,3-Dioxol-2-one 85 29 ' ■ i ■ ■ ' ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ‘ 3,60 3.80 4.00 4.20 5000 42 m/z 81.90 22.39% 14 58 17 0 • ■ i' ■ THTT 26 32,381 64 71 448,53, 9-7 miz-> Abundance 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 29 #541: Formamide, N-(cyanomethy!)- 3.60 [MMAMAAAAMAL 3.80 4.00 4.20 m/ z 43.10 19.90% 84 55 5000 40 36 43 5861 66 0 "TI’ *« 11111 * * * * I * * * * 1111 +HHT IP ■ ■ । ‘ ‘ । ■ • ■ • । ■ t ‘ ।' Ti/Z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.60 3.80 4.00 4.20

12162.D 052202.M Wed May 29 09:55:12 2002 Page 9

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