GCMS calculation results for sample AE11602, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052802\11602.D Vial: 8 Acq On : 28 May 2002 8:00 pm Operator: McLean Sample : 5/24 ad re-ext Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) AE- Title : 508 Modified.GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 7 1,3-Dioxol-2-one Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 3.95 0.50 ug/L 328015 1,4-Dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3-Dioxol-2-one 86 C3H203 000872-36-6 5 2 Crotonic acid 86 C4H602 003724-65-0/4 3 Crotonic acid 86 C4H602 003724-65-0 4 4 2-Butenoic acid, (E)- 86 C4H602 000107-93-7 4 Abundance Scan 147 (3.943 min): 11602.D (-146) (-) m/z .86.00 100.00% 85

49 5X0 82 39 ' ■ I ' ‘ ‘ ' I ‘ ‘ I ‘ ‘ I ‘ ‘ ' I ■ 36

niz-> 01 5 m- ■111 ■ 10 15 20253035404550556065 70 75 80859095 mm -mmp 3.X m/z 3.X 49.10 4.X 4.20 61.91% Abundance #116747: 1,3-Dioxol-2-one 29 85

42 5000 ’114’1111 T V 3.60 3.804.X 4.20 58 m/z 84.00 53.20%

HT]33944.50.55.—6 63 67 71 77 83 +89— n/z-> 0! — .... 27 32 3639 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ■' i ■ ■ “ i1 ■" i1" • i “ "i

Abundance #116766: Crotonic acid 41 85 ' ' i ■ ■ ‘ ■ i ' ‘ ‘ ■ i 1 ‘ ■ i • ‘ ■ i ‘ 3.X 3.X 4.X 4.20 5000 m/z 47.10 47.76% 69 .* 27 3£ 45 15

n/z-> 01 5+12118,,2413134 450535760...66412,,.. 1 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 1111'1" I “1

Abundance #116767: Crotonic acid ■ ■ । ■ ■ • ' i ■ ■ ■ ' i ■ ' ' ■ i ■ ■ • ■ i ■ 86 3.X 3.X 4.X 4.20 m/z 83.00 35.43% 41 5000 69 45 58 27, 38 0 ----- Ills”.............. po 9—7 * * i *1 ■ ’ ।1 * * * । * • ■ • । * ‘ ■ * ik miz-> 5 10 15 20253035404550556065 70 75 80859095 3.X 3.X 4.X 4.20

11602.D 052202.M Thu May 30 10:38:10 2002 Page 10

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