GCMS sample analysis results, AE11904, June 3, 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052202\11904.D Vial: 11 Acq On : 22 May 2002 9:58 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 4 1,3-Dioxol-2-one Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 3.80 0.63 ug/L 449680 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,3-Dioxol-2-one 86 C3H203 000872-36-6 9 2 1,3-Dioxol-2-one 86 C3H203 000872-36-6 9 3 1,3-Dioxol-2-one 86 C3H203 000872/36-6 9 4 l-Buten-3-yne, 2-chloro- 86 C4H3C1 017712-36-6 5 Abundance Scan 123 (3.802 min): 11904.D (-121) (-) m/z 86.00 100.00% 85 35 50 82 43 5000

58 3.40 3.60 3.80 4.00 4.20

miz-> MIU 0! ‘ ■ i ■ ■ “ i ■ “ ■ i' “ ‘ i ■ “' i • “ ■ i ■ ■ • 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 • “ • j • ■ TIOICTur ‘I ‘1’4*4114* m/z 50.05 70.50% Abundance #34604:1,3-Dioxol-2-one 85 29 42 5000 3.40 3.60 3.80 4.00 4.20 14 58 m/z 35.10 68.63% 17 0!Tppr TTmth 26 32.384 +4548,53+ 64 71 ■ 111 ■' ‘ 11 ■ ■ ■ i ‘ ■ ■ ■ i“' ■ i “' ‘ i 89- niz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #116747:1,3-Dioxol-2-one 29 85

42 3.40 3.60 3.80 4.00 4.20 5000 m/z 82.00 64.60% 58

0! 11/1111/2111/2111/2378 Huff 32 36391 f5.F9.F5.rf63 67 71 77 83 89-7 ।।i> t ■ 11.... ।... >, n/z-> Abundance 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 #116748: 1,3-Dioxol-2-one 85 ' 1 1 3.40 1 ' 1 1 3.60 3.80 J 4.00 4.20 29 42 5000 58

26 miz-s O ■.rjiiricnriii.nl.mil. ....... 1f548,57. 62 74 83 IMI—BB—2B2—B91118331 —p 1 i 1 1 ■ • i ■ • ■ ‘ i ■ • ■ ; i • ■ ■ ■ i 1 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.40 3.60 3.80 4.00 4.20

11904.D 052202.M Tue May 28 12:09:05 2002 Page 7

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