GCMS sample analysis results, AE11799, June 3, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052202\11799.D Vial: 6 Acq On : 22 May 2002 5:54 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e ?** Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 7 1,3-Dioxol-2-one Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 3.92 0.74 ug/L 593612 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,3-Dioxol-2-one 86 C3H203 000872-36-6 7/ 2 1,3-Dioxol-2-one 86 C3H203 000872-36-6/4 3 1,3-Dioxol-2-one 86 C3H203 000872-36-6 4 4 Crotonic acid 86 C4H602 003724-65-0 4 Abundance Scan 143 (3.919 min): 11799.D (-141) (-) m/z 86.00 100.00% 85

500) 35 47 50 58 ■ ■ i ' 1 1 ■ i4 1 ■ ■ i 1 1 1 ■ 1 1 1 ‘ ■ i

Tt/Z-> Of 1111111111111—111101111116117—HHI+38 43 1’111 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ..... 3.60 rn/z 3.80 35.10 4.00 4.20 44.61% Abundance #34604:1,3-Dioxol-2-one 29 85 Aw MWw M 42 5000 ■ ■ i ■ ‘ ■ 1 i ‘ ■ I ‘ 1 1 ■ i ■ • 1I 3.60 3.80 4.00 4.20 14 58 m/z 47.00 43.33% 17 01TITTTTTUTTT 26 32 38 ’I’1 8+44648,53+ 64 71 89—7 nz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #116748:1,3-Dioxol-2-one 85 29 I*1’**’I’***I***’I 42 3.60 3.80 4.00 4.20 5000 m/z 86.90 28.70% 58 N 26 l 4548 55 62 74 83 0 TTTTTTTTTT# -rm-p-rTHpt m/z-> 5 10 15 20253035404550556065 70 7580859095 Abundance 23 #116747:1,3-Dioxol-2-one 85 Per I11) "iet dr 3.60 3.80 4.00 4.20 m/z 50.00 25.78% 42 5000 58

/z—> 01 „.. 32 3639 tp +46-50.55.46 63 67 71 77 83 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 89.7 3.60 3.80 4.00 4.20

11799.D 052202.M Tue May 28 12:02:52 2002 Page 10

NYC-WTC_000012808