GCMS analysis results for sample AE12162, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C: \MSDCHEM\ 1 \DATA\052302\12162.D Vial: 15 Acq On : 23 May 2002 9:22 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 8 Propiolonitrile Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T.

4.23 0.22 ug/L 135254 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Propiolonitrile 51 C3HN 001070-71-9 5 2 Methane, chlorodifluoro- 86 CHC1F2 000075-45-6 4 3 2-Chloroethanol 80 C2H5C10 000107-07-3 4 4 2-Chloroethanol 80 C2H5C10 000107-07-3 2 Abundance Scan 196 (4.231 min): 12162.D (-194) (-) m/z 51.10 100.00% 51

5000 35 41 84 88 "d 47 3.80 4.00 4.20 4.40 4.60 O+ ITT ■ i ■ ■ " i" " i ‘1 “ i “ “ i - TH ■ i ■ ■ ‘ ■ i ■ ■ m/z 88.00 53.82% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #12371: Propiolonitrile 51

5000 3.80 4.00 4.20 4.40 4.60 m/z 49.10 47.33%

miz-> • 01 5+12.18, 428,32.38,+47 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 —-—"“—22—10

Abundance #111064: Methane, chlorodifluoro- 51 3.80 4.00 4.20 4.40 4.60 5000 m/z 84.00 43.32%

67 13 19 24 2831 3538 43 47 , | , 8588 O+ TTPTTTTTTHTTIT NO—tW —HpT n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #108328:2-Chloroethanol i ' ■ ■ ■ i ' ' ■ ■ I • ■ ■ ■ i ■ ■ ■ ' i • ■ 1 31 3.80 4.00 4.20 4.40 4.60 m/z 41.10 33.40% 5000 27 44 . 49 353841 ,,153 576063 76 80 0: 1’1591101115111170021111 Httmppm m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.80 4.00 4.20 4.40 4.60

12162.D 052202.M Wed May 29 09:55:12 2002 Page 10

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