GCMS analysis results, sample AE12479, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052902\12479.D Vial: 21 Acq On : 30 May 2002 2:22 am Operator: McLean Sample : gc/ms scan 5/28 fb Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 6 Propiolonitrile Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T.

3.89 1.24 ug/L 856504 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Propiolonitrile 51 C3HN 001070-71-9 3/ 2 Methane, chlorodifluoro- 86 CHC1F2 000075-45-6 2 3 Ethane, 1,1-difluoro- 66 C2H4F2 000075-37-6 2 4 2-Chloroethanol 80 C2H5C1O 000107-07-3 1 Abundance Scan 138 (3,890 min): 12479.D (-134) (-) m/z 51.10 "0000 51

5000 e 36 86 47 58 40 83 1 1 I 1 1 1 1 i T ■ ■ i 1 ■ ■ '

3,60 3.80 4.00 4.20 0- TT ■"•I" +1-4*4’1+418*8*1888*184 '‘ l‘ “ ‘ I ‘' m/z 36.10 37.61% nz-> 0 5 10 15 20 25 3035404550556065 70 75 80859095 Abundance #12371: Propiolonitrile 51

5000 3.60 3,80 4.00 4.20 m/z 86.00 35.69% ... .................... . 0- i.. j.।...j t।(. iz-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #12363: Methane, chlorodifluoro- 51 3.60 3.80 4.00 4.20 5000 m/z 47.10 27.29%

31 :35 67

niz-> 0- 13 19 24 TPmmmppght 0 | mm 47 , 54 ,| ,________ 85 i.. j।. 11111j.... ।.. i...... 11 > i. ।।. 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #111062: Ethane, 1,1-difluoro- 51 3.60 3.80 4.00 4.20 m/z 58.10 25.07% 5000 65

47 15 27 31

vfz-> 0 -,2.,192413124...43l. tppt i।j... i।।. 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 411 3.60 3,80 4.00 4.20

12479.D 052202.M Mon Jun 03 11:41:43 2002 Page 9

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