GCMS analysis results sample AE11926, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052302\11926.D Vial: 6 Acq On : 23 May 2002 2:02 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 4- Borane, trifluoro­ Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

3.80 0.67 ug/L 475395 1,4-Dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Borane, trifluoro- 68 BF3 007637-07-2 2 2 2-Chloroethanol 80 C2H5C1O 000107-07-3 2 3 Boron trifluoride etherate 142 C4H10BF3O 000109-68-7 2 4 2-Chloroethanol 80 C2H5C1O 000107-07-3 2 Abundance Scan 123 (3.802 min): 11926.D (-121) (-) m/z 49..10 100.00% 49

5000 43

0- 7 58■ i ■ ■ ■ ■ i • ■ ■ ■ i ■ 85 3.40 m/z 3.60 51.10 3.80 4.00 4.20 38.62%

.PMa • ■ ■ i ■ ■ • ' i ■ ■ ■ ■ i 11■ ■ i ■ ■ ■ • i ■ ■ ‘ ‘ I ' ' ' ' I ' miz-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #12321: Borane, trifluoro- 49

50001 3.40 3.60 3.80 4.00 4.20 m/z 48.10 33.40% 11 1,9 30 38 68

niz-> 0- —nm i1" ■ n

Abundance 0 10 20 30 40

31 50 60 70 80 90 #108328: 2-Chloroethanol 100 110 120 130 MAWMpwtw 3.40 3.60 3.80 4.00 4.20 5000 m/z 43.10 24.84% 44 ___

0- ■ • i ' ■ ■ • i ■ ■ ' ■ i 37,1441,57,63. T1000— 80 aBuamuT**maPpu3r n/z-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #1099: Boron trifluoride etherate 31 3.40 3.60 3.80 4.00 4.20 m/z 42.00 12.94% 59 5000 45 74

0- ■ ■ । ■ 15.25 1Ir 39444——— I'1 "66' l, .81 93 -127— /z—> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 3.40 3.60 3.80 4.00 4.20

11926.D 052202.M Wed May 29 09:47:50 2002 Page 7

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