GCMS analysis results sample AE11926, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052302\11926.D Vial: 6 Acq On : 23 May 2002 2:02 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 3 Crotonic acid Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 3.76 0.81 ug/L 571737 1,4-Dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Crotonic acid 86 C4H602 003724-65— 9 2 cis-3-Hydroxy-dl-proline 131 C5H9NO3 1000132-83-9 9 3 2-Butenoic acid, (E)- 86 C4H602 000107-93-7 7 4 Isocrotonic acid 86 C4H602 000503-54-0 7 Abundance Scan 116 (3.761 min): 11926.D (-114) (-) m/z 86.00 100.00% 86

5000 49

42 58 3.40 3.60 3.80 4.00 4.20

miz-> Of 20 30 mm 40 50 60 70 80 1 1 IA"O"T . . r । i i i . j . . , , । . i . i ] 90 100 110 120 130 m/z 49.10 40.06% Abundance #116767: Cratonic acid 86 41 5000 69 3.40 3.60 3.80 4.00 4.20

ProsMHruyy m/z 87.95 19.49% 97 58

miz-> 01 20 +1l15 1. ■ ‘ 1 ■ ' PP 30 40 50 60 70 80 •mOP—C—T 90 100 110 120 130 Abundance #34657: cis-3-Hydroxy-dl-proline 86 340 3.60 3.80 4.00 4.20 5000 41 m/z 84.00 17.41% 69

59 01 --47—7. DBTm—mmn—/——B—n/nOn—T . 92 113 131 miz-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #116768:2-Butenoic acid, (E)- 86 340 3.60 3.80 4.00 4.20 m/z 42.00 12.46% 41 5000 M 69

m/z—> 0 .20.....30341140450.57,63, I 50 60 1’1 70 1 75 I ‘ ■ 80 90 —PP 100 110 120 130 • * i ■ ■1 3.40 । • ■ • ■ । ‘। 3.60 3.80 4.00 ■ i ■ 4.20

11926.D 052202.M Wed May 29 09:47:50 2002 Page 6

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