DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB26\02086.D Vial: 3 Acq On : 26 Feb 2002 4:27 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 26, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 5.95 0.32 ug/L 156904 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

13-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 36 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 36 3 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 4 2-Methyl-5-hexen-3-ol 114 C7H140 032815-70-6 9 Abundance Scan 228 (5.948 min): 02086.D (-) m/z 73.10 100.00% 73

5000

43 1 1 i ■ 1

57 87 5.60 5.80 6.00 6.20 11 TTTTTTLTTTUTTTUTTUTTTTTTTTPTTTTWWTTTT 0- 111 ■' " i ■ " ' i ■ ■ " i,T| ■ i ■1 "I' ‘' 'T m/z 43.10 24.47% Tl/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 4./A 5.60 5.806.00 ' ' i ' ‘ 6.20 . A ' I '

43 m/ z 41.10 11.37% 2755 , 87 113 174 0-— ' i " " i'' " 11i 1*01 —0011—0010000—0000—pm-01m0TTir m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 5.60 5.80 6.00 6.20 5000 m/z 45.0.0 9.31% 43 27 55 , 87 113 174 0- TTTT T4 11" " 11" 'T1 1" i " 1' i " " i " " iri' ‘ r " 111 " 11" " i " " 111 " 1111111 n/z- > 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... 30 5.60 5.80 6.00 6.20 73 m/z 71.00 8.24%

5000 44 58 15 - m/z-> 0 H10yPAgual '11" 1111" i " " i11 ,ri1"111111111111"1 ■ i " " i' " 11" " i " " i1 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

02086 .D HP022102.M Wed Feb 27 08:35:01 2002 Page 8

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