GCMS instrument data file SCAN508, Jan 31 2002

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Instrument output file from GCMS analysis using method SCAN508 showing response for deuterated internal standards.

NYC-WTC_000052205–000052221

Folder label: “GCMS X 1/11/02 A 1/31/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN31\00845.D Vial: 6 Acq On : 31 Jan 2002 6:51 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 1 3 -(CYCLOHEX-3'-EN-YL)PROPAN. .. Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

5.93 0.35 ug/L 165017 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3 -(CYCLOHEX-3 ’-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 36 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 36 3 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 4 Propane, 2-methoxy-2-methyl- (CA... 88 C5H120 001634-04-4 9 Abundance Scan 224 (5.931 min): 00845.D (-) m/z 73.10 100.00% 70

5000 — 43 1 1 i ' 1 TTI 5.60 5.80 6.00 6.20 m/z—> . .................1 —l 55 1l ■ । ■ ■' ■ । ■ ■ ■1 r' |...... 87...... 103........................................................ 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 m/z 43.10 23.90% Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 70

5000 CInnn 1107’ , । . TTrrT 5.60 5.80 6.00 6.20 43 m/ z 41.10 9.69% 27 55 , 87 113 174 a 0000—ma00—*me*mBn—uTTO—TTnIr 0- ........... igimm ’4 TTTTUTTT m/z~> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 70 -A 5.60 —AMA— 5.80 6.00 6.20 5000 m/ z 45.10 9.26% 43 27 55 , |...... 87.............. 113........................................ 174 01111" " r i1 T m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... 30 5.60 5.80 6.00 6.20 73 m/z 71.1.0 8.11% 5000 44 58

m/z-> 0 M - TTTTTTTTTTUTTm 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

00845.D SCAN508.M Fri Feb 01 09:19:34 2002 Page 3

NYC-WTC_000052209

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