GCMS analysis results for sample AE00320, Jan 2002

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Laboratory report showing GCMS analysis of sample AE00320 for unknown compounds and DDD on January 10, 2002.

NYC-WTC_000051137–000051151

Folder label: “GCMS X 1/7/02 A 1/8/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

. Data File : C: \MSDCHEM\1\5973N\02JAN08\320.D Vial: 5 Acq On : 8 Jan 2002 8:47 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.89 5.45 ug/L 1884360 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 J3 3 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 4 1,3-Dioxolane, 2-pentadecyl - $$ ... 284 C18H3602 004360-57-0 9 Abundance Scan 220 (5.885 min): 320. D (-) m/z 73.10 100.00% 73

5000 43 5.60 5.80 6.00 6.20 55 . 87 103 m/z-> 01 ............ 1 ' I ■' " I' 11 ' 11 *0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 m/z 43.10 23.87% Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 5.60 5.80 6.00 6.20 43 m/z 45.10 9.10% 27 87 55 113 174 nr1 . ............'I N-rreme ■ I 01 i ’''' I ’' ’' I TVT) III" nz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 ——*——00111111* 5.60 5.80 6.00 6.20 5000 m/z 41.10 9.00% 43 27 55... 113 87 174 n/z-> .... 01PpWpPm ' I " " I' " ' I ’ 1’1 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 । ■1 ■11 i'''' i ■ ■ " i ■ ■'' i r " ' i'

Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... 30 5.60 5.80 6.00 6.20 73 m/z 71.10 6.64% 5000 44 58

m/z-> 0 J ‘ ‘‘I An 1...... ...... I • ■ ■ * i11 •' i • " ' r ■ ■' i 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 I" 111"111 i' " ' r 5.60 5.80 6.00 6.20

320.D SCAN508.M Wed Jan 09 15:18:12 2002 Page 7

NYC-WTC_000051147

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NYC-WTC_000051147Source: NYC Law Department, mirrored locally

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