GCMS analysis results for sample AE00843, Feb 4 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\1\5973N\02JAN31\00843.D Vial: 5 Acq On : 31 Jan 2002 6:01 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

5.93 0.34 ug/L 189474 1,4 -Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

13-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 28 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 28 3 1,3-Dioxolane, 2-heptyl- 172 C10H20O2 004359-57-3 25 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 224 (5.931 min): 00843.D (-) m/z 73.10 100.00% 73

5000 43 ■ • i ■ ■ ■ ■ i ' ' ' ■ i ' r ■ ■ i ' ' ’ ■ i 5.60 5.80 6.00 6.20 0 -4 .55... 11 +p 87 •i■■■ ■ i ■ ■' 'i1 103 ■ ■ • i ■ ■ ■ ■ i' i1 ■ ■ ■ i ■ ■'' i ■ ■ ■ • i ■ ■' ■ i ■ ■ ■ ■ i ■1111 Tr m/z 43.10 25.33% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 7t3

5000 — fTrT "I 5.60 5.80 6.00 NV 6.20 43 m/z ‘45.10 9.71% 27 55 , 87 113 174 01■ i • ■' ■ i1 —04PPT 4TT P T 1119199211029’ i ■ ■ ’ ■ i' n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 5.60 5.80 6.00 6.20 5000 m/ Z 41.10 8.39% 43 27 55 87 113 174 0- 11"111 r "11'111 ■ i " ■ ■ r ' ■' i ■ 1Ir ■ I■ ■ I........ l1" ■ i' m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #76647:1,3-Dioxolane, 2-heptyl- .......................... 78 5.60 5.80 6.00 6.20 m/ Z 71.10 7.24% 5000

45 27 ............ 57 99 171 .................. /z--> oV ' ■ ''i ■ • 1..... ..111111r 20 30 40 50 60 441 i ■ ■ ■ ■ r i' ■' ■ i1 ■'' i' ■'' r '' ■ i'' ■ ■ i ■ ■ ■11' ■ ■ ■ i' 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

30843.D SCAN508.M Fri Feb 01 09:19:27 2002 Page 7

NYC-WTC_000052138