GCMS analysis results for sample AE00833, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN31\00833.D Vial: 1 Acq On : 31 Jan 2002 2:42 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ****************************************************** *********** * *** Peak Number 5 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

5.92 0.47 ug/L 248847 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

13-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 45 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 45 3 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 4 Propane, 2-methoxy-2-methyl- (CA... 88 C5H12O 001634-04-4 9 Abundance Scan 223 (5.920 min): 00833.D (-) m/z 73.10 100.00% 73

5000

43 5.60 5.80 6.00 6.20 1 I 55 1 । 87 103 01.............. TTTTTTTTTTT TTTI’ -1 > । ■ i ■ • ■ ■ ir m/z 43.10 21.11% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 PIluv 1 ”i ' 1 1 It ri । . । .. । 5.60 5.80 6.00 6.20 43 m/z 41.10 8.96% 27 55 87 113 174 0 iij......... privet ■ i ■ ■ " i" ' ’.I’i — TIPwmU I " " I " " 11 " 11' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 A .................... A 1 5.60 5.80 6.00 6.20 5000 m/z 45.10 8.36% 43 27 55 । 87 113 174 o1'' i " ' ■ 11 " 111 TTTT 'I1'1...... 1 i 11' n I ■'1' 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... ■ ■ ■ i 1 ■ • ■ i ■ ' ■ ■ i ■ ■ ■ ■ । 1 1 ' ■ i 30 5.60 5.80 6.00 6.20 73 m/z 71.10 7.38% 5000 44 58

15

n/z-> 0 7 ..... W..... 'I " 111'1 1111 ri 1 rr ri 111111111111111' f''" r ''' i' " ' i'' " i' " ' I' 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 ■ ■ । ■ • ■ • । • ■ ■ ■ । 5.60 5.80 6.00 ‘ । । 6.20 ।

00833.D SCAN508.M Fri Feb 01 09:18:59 2002 Page 7

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