GCMS analysis results for sample AE00843, Feb 4 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\1\5973N\02JAN31\00843.D Vial: 5 Acq On : 31 Jan 2002 6:01 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 l-Hexene, 6-bromo- (CAS) $$... Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

4.87 0.08 ug/L 42047 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Hexene, 6-bromo- (CAS) $$ 6-Br... 162 C6HllBr 002695-47-8 9 2 1-Hexene, 6-bromo- 162 C6HllBr 002695-47-8 9 3 1-Propenylaziridine 83 C5H9N 000000-00-0 7 4 (Z)-1-Propenylaziridine $$ Aziri... 83 C5H9N 024461-38-9 7 Abundance Scan 131 (4.869 min): 00843. D (-) m/z 84.05 100.00% 41 84 55

5000

4.60 4.80 5.00 5.20 ol ■ I '''' I' TTr i • ■ ■' i ■ • ■ ■ i ■ • ■ ■ i ■ ■ ■' i ■ ■ ■' i m/z 41.10 88.49% m/z-> 20 30 40 50 90 100 110 120 130 140 150 160 170 60 70 80 Abundance #61499:1-Hexene, 6-bromo- (CAS) $$ 6-Bromo-1 -hexene $$ 1-... 41 55

5000 27 67 83 ....... h..... 4.60 4 80 5.00 5.20 m/z 55.10 73.59% 162 0 ' I '' '' I' ' ' ' I ' ' ' ' I ' • i'1 • ’ i ■ • ■ ■ i Tl/Z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #61496:1-Hexene, 6-bromo- 41 55 83 4.60 4.80 5.00 5.20 5000 m/z 39.10 59.33% 27 67

136 162 0 ' i " '' i'1'' i1 '' i'11' i' " 11 *1]—nuIp——BIpuunm——mmaTIHTT m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #3036:1-Propenylaziridine 41 55 4.60 4.80 5.00 5.20 83 m/z 83.00 52.33%

5000 27

68

m/z-> 0 ■ i • ■ ' i ■ ■'' i 20 30 40 ' ■ i' 50 | L60 v ।■ i1' ■ ■ i ■' • ■ i'' 1 ' i ■ ■ ■ • r ' ■' i'1'' i

70 80 90 100 110 120 130 140 150 160 170 IT’II"1 4.60 4.80 5.00 5.20

30843.D SCAN508.M Fri Feb 01 09:19:27 2002 Page 6

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