GCMS analysis results for sample AD31585, Jan 28 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\O2JAN17\31585.D Vial: 1 Acq On : 17 Jan 2002 2:50 pm Operator: Sample : 508 scan Inst. : Instrumen Mise : January 17, 2002 Multipir: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 1-Hexene, 6-bromo- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 4.85 0.18 ug/L 50415 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Hexene, 6-bromo- 162 C6HllBr 002695-47-8 12 2 4-Pentenal (CAS) $$ 4-Pentenal- 84 C5H80 002100-17-6 9 3 1-Hexene, 6-bromo- 162 C6HllBr 002695-47-8 9 4 1-Hexene, 6-bromo- (CAS) $$ 6-Br... 162 C6HllBr 002695-47-8 9 Abundance Scan 129 (4.846 min): 31585.D (-) m/z 84.00 100.00% 84 55 41 5000 AVWW i ■ ■ ■ ■ i ‘ ‘ ■ i • ■ • ■ i • ■ ‘ ■ i ■ ■ • 4.40 4.60 4.80 5.00 5.20 01 ■ H 1 ‘ ‘ ‘ l " ' ' I ‘ ‘ ‘ I ‘ ‘ I' ' ■ ‘ I ' ■ ‘ ‘ I ‘ ‘ ‘' I ‘ ‘ ‘ 11 ‘ m/z 55.10 68.11% miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #61496:1-Hexene, 6-bromo- 41 55 83 5000 27 i ‘ 1 1 ‘ i ■ ■ ■ ■ i ■ ■ ’ ■ i ■ ■ ■ ■ i ■ ' ■ 67 4.40 4.60 4.80 5.00 5.20 m/z 41.10 56.19% 136 162 Of • । ■ ■ • • । • - 11 • • ■।• ■■i“ i1 ■ ■ ■ i ........... . I.... I»... 111.. 1. miz-> 20 30 40 50i 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #3205:4-Pentenal (CAS) $$ 4-Pentenal-

27 39 55 83 —M . . 4.40 m/z 4.60 83.00 4.80 5.00I 5.20 i48.33% 5000i

mfz-> Abundance 0! 20 30 40 m HH50 60 69 " । ■1 ■ ‘ । । ■ ■ ■ * । 70 80 90 100 110 120 130 140 150 160 170 #61497:1-Hexene, 6-bromo- ■ i “ ■ ■ । ‘। ■111 ■ ■11 ■

i ■ ' ■ ■ i ■ ■ ■ ■ i ■' ■ i ‘ • ■ • i ■ ■ ■

41 4.40 4.60 4.80 5.00 5.20 m/z 39.10 46.92% 83 5000 27 67 y n/z-> 0 ‘ 11 ‘ • I ‘ ‘ *11 20 30 40 JU 11 ‘ • I 162 50 60 70 80 90 100 110 120 130 140 150 160 170 134 ■" । ■1 “ । ■ ■ ■ ■ । ।11'111 4.40 4.60 4.80 5.00 5.20

31585.D SCAN508.M Tue Jan 22 08:36:51 2002 Page 4

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