DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB26\02016.D Vial: 4 Acq On : 26 Feb 2002 12:49 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 6, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 5.95 0.27 ug/L 141356 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

13-(CYCLOHEX-3 7-EN-YL)PROPANOL $$. . . 174 C8H14O4 015745-87-6 40 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 40 3 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 4 l-Hexanol, 6-amino- $$ l-Amino-6... 117 C6H15NO 004048-33-3 9 Abundance Scan 228 (5.948 min): 02016.D (-) m/ z 73.10 100.00% 73

5000

43 . ........................ . .. ।. r > ■ ■ ■ । ■ 5.60 5.80 6.00 6.20 55 ‘'111 '' I 87 I 1'1, O-T 11 " 11 1 ‘' 1I 1111 " 1' i' " ' i " " i " 1 ‘ i " " i " " r 1 " i ‘ ' i" " i " " r m/z 43.10. 23.34% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 '

5000 ' ' i ' ' ‘ ■ i 1T1 ' 1 1 1 1 5.60 5.80 6.00 6.20 43 m/z 45.10 9.41% 27 55 , 87 113 174 0rp 11 > 111 ' 111 i i m I'lh'i 1 r ■ ■11 " 1»r> Ius’uds,’tIt’t’!....... 11111111111111111111111111 > 11111 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 5.60 5.80 6.00 6.20 5000 m/z 41.10 9.31%

43 27 174 0- TT ’+’554*11’41 ' i' ,' " r ■871 ■ i'1" i " '' 113 ——I.,— i " i‘ ' I'1'1 r ‘ " i111111' " 11 " 111 m/z- > 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... 3b 5.60 5.80 6.00 6.20 73 m/z 71.0.0 5.67% 5000 44 58

15 0 - Tp TTTTTTTTTTTTTTLTTTTTPTT ' 1 i ■ ' 1 ■ i 1 ■ ■ ■ i ■ ■ ■ ■ i 1 1 1 1 I ' m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

02016.D HP022102.M Wed Feb 27 08:34:32 2002 Page 8

NYC-WTC_000004536