DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000003981–000004147

Folder label: “GCMS X 1/29/02 A 2/1/02”

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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB01\31218.D Vial: 4 Acq On : 1 Feb 2002 5:13 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ************************************************** ** * * ******** * * * * * * * Peak Number 3 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

5.93 0.45 ug/L 193251 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

13-(CYCLOHEX-3 ’-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 36 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 36 3 Pentanol, 5-amino- 103 C5H13NO 002508-29-4 9 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 224 (5.931 min): 31218.D (-) m/z 73.10 100.00% 73 A

5000

43 ......................................... 1 1 । ■ ' ■ 1 i ■ ■ ■ 1 । 1 ■ ■ ■ । 1.. 87.. 103....................... 55 5.60 5.80 6.00 6.20 0- .. r 44 44 TITTTT —++ m/z 43.10 24.19% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 1 1 i ' ' TIPA 5.60 5.80 6.00 6.20 43 m/ z 41.10 9.82% 27 55 87 113 174 0--- ■ 11 ■ ■ 11 ■ ■ 11 |i +) ■ । ■ • ■ ■ i ' > ■ ■ । । ■ ■ ■ ■ । ■ < < • । ■ i । । ■ ■ > ■ । > 1 • ■ । ■ miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 A4 5.60 5.80 6.00 6.20 5000 m/z 45.10 8.66% 43 27 55 87 113 174 01TTTTTT ■ i " ‘ ■ ir ■ ■1T' 11111 II‘‘+‘I‘414111*‘1‘*‘*I+‘‘‘I‘‘I‘1‘1/+I+-I‘‘‘41* niz- > 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #9904: Pentanol, 5-amino- ■ ' I ' ' ' ' I 33 5.60 5.80 6.00 6.20 m/z 71.10 6.02%

5000

, 43 56 67 85 103 OTTT ■ ' । ■ 1 1 ■ i 1 ■ ■ ■ i ■ 1 ■ 1 । ‘ । /z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

31218.D SCAN508.M Mon Feb 04 08:41:42 2002 Page 5

NYC-WTC_000004059

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NYC-WTC_000004059Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999