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GCMS analysis results for sample AE00100, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE00100 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050354–000050369

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN23\00100.D Vial: 3 Acq On : 23 Jan 2002 4:36 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 Nonane $$ n-Nonane $$ Shell... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 9.45 0.14 ug/L 50302 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Nonane $$ n-Nonane $$ Shellsol 1... 128 C9H20 000111-84-2 53 2 Nonane, 2-methyl- (CAS) $$ 2-Met... 142 C10H22 000871-83-0 47 3 Nonane (CAS) $$ n-Nonane $$ Shel... 128 C9H20 000111-84-2 42 4 Nonane (CAS) $$ n-Nonane $$ Shel... 128 C9H20 000111-84-2 42 Abundance Scan 532 (9.447 min): 00100. D (-) m/z 57.10 100.00% 57 43

5000 71 85 281 —r1 ' i 1 ' 1 1 r'1 1 ' I ' — 9.00 9.20 9.40 9.60 9.80 0- 1***‘I** > ■ ■ ■11 ■ ■ ■ ■ i • ■ ■' i ■ • ■ ■ i ■ ‘ ■11 • ‘ ■1 r''1111'1 11'11 1111111'11 ' 11 rn/z 43.10 79.30% miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #25147: Nonane $$ n-Nonane $$ Shellsol 140 $$ n-C9H20 $$ U... 40 57 5000 _AA 9.00 9.20 9.40 9.60 9.80 27 71 85 m/z 41.10 27.47% 99 128 5 i ■ ■ ■11' ■ 1'1 ■ i 4.......... . ............. .. ............. .............. n/z—> 3) 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #38822: Nonane, 2-methyl- (CAS) $$ 2-Methylnonane $$ 2-Met... 43 57 9.00 9.20 9.40 9.60 9.80 ' 5000 m/z 71.10 25.98% 71

27 II, i .• ‘il 1 '............................................................. ..................................... 0V i ' ‘ ‘ ‘ I ‘ ‘ ‘ ■ i ■ ‘ ‘ 11 ■ ■ ■ ■ i ■ 1 ■ ■ i • ■ ■ ■ i ■ ‘ ‘ i ■ • ■ 1 11 ' ' 1 1 11 1 1 111 nz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #25153: Nonane (CAS) $$ n-Nonane $$ Shellsol 140 $$ n-C9H2... 40 57 9.00 9.20 9.40 9.60 9.80 ' m/z 85.10 25.30% 5000 71 85 99 128 O-TTTT 1 11111 L‘11______ 1____________________________________ ‘111111/31/1111113-0-" ‘‘Tr23113S32—33311TT11T 0s n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 9.00 9.20 9.40 9.60 9.80

00100.D SCAN508.M Thu Jan 24 09:57:10 2002 Page 7

NYC-WTC_000050364

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NYC-WTC_000050364Source: NYC Law Department, mirrored locally

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