GCMS analysis results for sample AD31646, Jan 25 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN22\31646.D Vial: 2 Acq On : 22 Jan 2002 1:02 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 Nonane $$ n-Nonane $$ Shell... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T.

9.45 0.13 ug/L 42730 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Nonane $$ n-Nonane $$ Shellsol 1... 128 C9H20 000111-84-2 72 2 Undecane (CAS) $$ n-Undecane $$ ... 156 C11H24 001120-21-4 72 3 Nonane (CAS) $$ n-Nonane $$ Shel... 128 C9H20 000111-84-2 72 4 Undecane 156 C11H24 001120-21-4 72 Abundance Scan 532 (9.447 min): 31646.0 (-) m/z 57.10 100.00% 43 57

5000

| 71 85 281 -444 9.20 9.40 9.60 9.80 9.00 14444 r !aa)koo)**0*/GG m/z 43.10 96.32% nZ—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #25147: Nonane $$ n-Nonane $$ Shellsol 140 $$ n-C9H20 $$ U... 43 57 5000 i ■ ■ ■ ■ i ■ ■ 9.00 9.20 9.40 9.60 9.80 27 71 85 m/z 41.10 42.36%

iz—> 20 -f 60 100 120 40 220 260 28080 140 160 180 200 240 Abundance #56237: Undecane (CAS) $$ n-Undecane $$ Hendecane $$ n-C11... 43 57 9.00 ' 9.20 9.40 9.601 9.80 5000 m/z 71.10 36.50% 71 85 A —— 98 113 156 ■’i ■ ■ ‘ ■ i ■ ■ ■ ■ i ■ ■ ■11 ■ • ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i' ■ • ■ i ■ ■

n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #25153: Nonane (CAS) $$ n-Nonane $$ Shellsol 140 $$ n-C9H2... T T 43 57 9.00 9.20 9.40 9.60 9.80 m/z 85.10 33.07% 5000

71 85 99 n/z—> 14 128 *a2*200*GG i • ■ ■ ■ i ■ •»11 > 20 40 60 80 100 120 140 160 180 200 220 240 260 280 9.00 9.20 9.40 9.60 9.80

31646.D SCAN508.M Thu Jan 24 13:55:34 2002 Page 6

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