GCMS analysis results for sample AE00830, Feb 2002

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Laboratory report showing GCMS analysis of sample AE00830 including surrogate recovery and unknown compounds.

NYC-WTC_000052047–000052068

Folder label: “GCMS X 1/11/02 A 1/31/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN31\00830.D Vial: 3 Acq On : 31 Jan 2002 12:11 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 2-Nonanone (CAS) $$ Methyl ... Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 4.91 0.08 ug/L 35869 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Nonanone (CAS) $$ Methyl hepty... 142 C9H18O 000821-55-6 9 2 2-Nonanone (CAS) $$ Methyl hepty... 142 C9H18O 000821-55-6 9 3 2-Isopropyl-5-oxohexanal 156 C9H1602 015303-46-5 9 4 3-Piperidinol, 1,4-dimethyl-, cis- 129 C7H15NO 037835-50-0 9 Abundance Scan 135 (4.915 min): 00830. D (-) m/z 43.10 100.00% 43 58

5000

71 84 207 —A . AM y5.204—- 4.60 4.80 5.00 0 'r11' I " " TT . ।।।■11 ■ 111 ■ ■ i "1 ■ r ■ " r' ” i" " i' " ' i1" ' r ■" i " 111" " r " 11" " i m/ z 58.10 67.63% m/z-> 20 30 40 50 60 70 80 90 100110120 130140150160170 180190 200 210 Abundance #38543:2-Nonanone (CAS) $$ Methyl heptyl ketone $$ Nonan-... 43 58

5000 1 1 1 i 1 ' 1 1 i ■ ' ■ 1 i 1 ' 1 1 i ' ■ 1 ' । 4.60 4.80 5.00 5.20 71 m/2 41.10 33.69% 85 99 113 127 142 0 TT TWWOTWOUUUgnum I" " 11' ‘1 i nn/z—> 20 30 40 50 60 70 80 90 100110120130140150160170 180190 200 210 Abundance #38535: 2-Nonanone (CAS) $$ Methyl heptyl ketone $$ Nonan-... 43 58 A ,/ -AALWA4 4.60 4.80 5.00 5.20 5000 m/ z 57.10 22.85% 27 71 85 99 114 127 142 01 ■ ।■ i ■ ■" i ■ ■ ■ • i ■ ’1 TWTTITmmumppaTu n/z-> :20 30 40 50 60 70 80 90 100110120130140150160170 180190 200 210 Abundancei #55578:2-lsopropyl-5-oxohexanal '"'I 1 1 ' 1 | 43 4.60 4.80 5.00 5.20 58 m/z 55.10 22.73%

5000 71 । 85 95 110 123 139

m/z-> 0 i ""i” "i -HHmm | rp-rr 20 30 40 50 60 70 80 90 100 110120130140 150160 170 180 190 200 210 4.60 4 80 5.00 5.20

30830.D SCAN508.M Fri Feb 01 09:18:31 2002 Page 4

NYC-WTC_000052054

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GCMS analysis results for sample AE00840, Feb 4 2002 · Box DEP Box 28

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Laboratory report showing GCMS analysis of sample AE00840 including surrogate recovery and unknown compounds.

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