GCMS analysis results for sample AE00830, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN31\00830.D Vial: 3 Acq On : 31 Jan 2002 12:11 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 3 3-Buten-2-ol, 2-methyl- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

5.02 0.22 ug/L 102231 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 72 2 Butenol, methyl- 86 C5H10O 060766-00-9 64 3 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 58 4 3-Buten-2-ol, 2-methyl- (CAS) $$... 86 C5H10O 000115-18-4 56 Abundance Scan 144 (5.018 min): 00830.D (-) m/ z 71.10 100.00% 43 71

5000 59 39 55 nk 84 4.60 4.80 5.00 5.20 5.40 01 IPmTPmTPI ----- m/ z 43.10 97.97% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #4083: 3-Buten-2-ol, 2-methyl- 71 43 A, , AN / y4 /A 5000 59 4.60 4.80 5.00 5.20 5.40 27 31 m/ z 41.10 63.65%

m/z-> 5 On ‘ ‘‘‘1111 TIT 37 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 mH ........ 36, Abundance #4093: Butenol, methyl- 43 71 / , A / WW —AA— 4.60 4.80 5.00 5.20 5.40 5000, 59 m/z 69.10 47.71% 15 27 31 53 1 671 86 01 " i" " i " " i' ‘TT "i"" i" -++++ . lily 1'" TT m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #4085: 3-Buten-2-ol, 2-methyl- r^ ■ ■ i ■ ■ ■ ■ । 1 ■ i ' ' 71 4.60 4.80 5.00 5.20 5.40 43 m/z 59.10 43.80%

5000 59 27 31 53 Of 11" •111"11r + " I'1 " I'1 86 THP II - 67, Kt A N M 1 1 I 1 11 1 1 11 ■ ' । 1 ' ‘I* 1 m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 4.60 4.80 5 00 5.20 5.40

00830.D SCAN508.M Fri Feb 01 09:18:31 2002 Page 5

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