GCMS analysis results for sample AE00100, Jan 2002

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Laboratory report for sample AE00100 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050354–000050369

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN23\00100.D Vial: 3 Acq On : 23 Jan 2002 4:36 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 2-Propanol, 1,1'-oxybis- (C... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 9.55 0.11 ug/L 41950 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, l,l'-oxybis- (CAS) $... 134 C6H1403 000110-98-5 40 2 2-Propanol, l,l'-oxybis- (CAS) $... 134 C6H1403 000110-98-5 40 3 2-Butanol, 3,3’-oxybis- 162 C8H1803 054305-61-2 9 4 2,3-Epoxy-3-methyl-6-methoxyheptane 158 C9H18O2 088083-53-8 9 Abundance Scan 541 (9.550 min): 00100. D (-) m/z 59.10 100.00% 59

5000 45 103 73 • ■ i ■ • ■ ■ i ■ ■ ’ I’ 86 9.20 9.40 9.60 9.80 0-___________ _____L i_______ ■ i ■ • ■ ■ i ■ ■ ■ ■ i ■ ■ ■ 1 i ■ ■ • ■ i ■ ■ ■ ■ i ■ m/z 45.10 40.74% mfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #29204:2-Propanol, 1,1 ’-oxybis- (CAS) $$ Dipropylene glyc... 59

31 5000 45 —■ ■ i1 ■ ■ ■ । ‘ ■ i ■ 1 1 ■ i• ■ • "IT 103 0.20 9.40 9.60 9.80 m/z 103.10 32.18% 0- T1ddnumB)mB——u—tunu—]unBBuIr miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #29205:2-Propanol, 1,1'-oxybis- (CAS) $$ Dipropylene glyc... 50 .............................................. 31 0.20 9.40 9.60 9.80 5000 45 m/z 73.10 22.70% 103

iz-> 1 0 TTT00m-n1-1———1—00—0001TT3-th———0oTm—t—uu1—0—T33IIr

Abundance 20 30 40 50 60 70 80 90 100 110 120 130 140 #61826:2-Butanol, 3,3’-oxybis- 50 .. M m/z 9.20 9.40 41.10 9.60 9.80 21.18% 5000- 31 45 103

O—TTT 14 I1" " r+les ' i'1111T1 •11 ■' ■' । ■ ■ ■' । • ■' ■ । ■1 ■ ‘ । ‘ 134 ' । ■1 ■ ■ । ■1 ■ ■ । ■ ■ ■ ।1 ■ ■ ■ i • ‘ ■ 1 । ■ • • • i ■ m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 9.20 9.40 9.60 9.80

00100.D SCAN508.M Thu Jan 24 09:57:10 2002 Page 8

NYC-WTC_000050365

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NYC-WTC_000050240

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