GCMS analysis results for sample AE00100, Jan 2002

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Laboratory report for sample AE00100 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050354–000050369

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN23\00100.D Vial: 3 Acq On : 23 Jan 2002 4:36 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1. . .\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 3-Cyanocarbazole $$ 9H-Carb... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T.

22.28 0.15 ug/L 91894 Phenanthrene-dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 64 2 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 59 3 2-CYANOCARBAZOLE $$ 9H-Carbazole... 192 C13H8N2 057955-18-7 50 4 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2: 000000-00-0 49 Abundance Scan 1656 (22.280 min): 00100.D (-) m/z 192.10 100.00% 1912

5000

_ 96

m/z-> 49 O —Ipp 1 70 82Pp m— .......11710..... ,i 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60 m/z 193.10 18.04% Abundance #103424:3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192

- 5000 11 1 ■ ■ • r 22.00 22.20 22.40 22.60 96 164 m/z 146.10 16.98%

mfa-> 138 0 ■ ■ i " • ■ i1 “ ■ i ■ ■" i " ■ ■ i “ “ i ■ ■' ■ i “ ■' i ■ ■1 ■ r ■■ ■ i " ■11' " ■ i ■ ■ • ■ i' 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 l "IT

Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 1112 .... A - ■ ‘ i ■ ■ ■ ■ i 1 • ■ 1 i ' 22.00 22.20 22.40 22.60 5000 m/z 191.10 16.48%

96 165 88 ,l 139 152 176 0 “ i1 ■ " i1 ■ “ 11 ‘" i1 “11 ‘ “11 ‘1' ■ i" ' ■ i “'' i ■ “ ‘ i ■ “ '"i ■"' i1 “ ■ i l IUpt 111 n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103420:2-CYANOCARBAZOLE $$ 9H-Carbazole-2-carbonitrile (CAS 192 ‘ 22.00 22.20 22.40 22.60 m/z 96.00 16.15%

5000

96 164 138 — 0 '11“ ■11“'■i■1"i■■ ■ ■ i1 ■■■i1 ■ i■ “■ i■ ■1 ■ i■ ■ ■ ■ i■ —H Tgm 1 ' I ' 1 1 ' M ' 1 1 1 1 ' 1 If| ' n/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

00100.D SCAN508.M Thu Jan 24 09:57:10 2002 Page 9

NYC-WTC_000050366

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