DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004494–000004704

Folder label: “GCMS X 1/30/02 A 2/26/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02FEB26\02086.D Vial: 3 Acq On : 26 Feb 2002 4:27 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 26, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 11 3-Cyanocarbazole $$ 9H-Carb... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.14 ug/L 118007 Phenanthrene-dl0 22.64 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 64 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 58 3 1,3-Benzodioxole, 4-methoxy-6-(2... 192 C11H1203 000607-91-0 53 4 N-(2-methylprop-2-enyl)-2-nitrob. .. 192 C10H12N2O2 000000-00-0 47 Abundance Scan 1675 (22.283 min): 02086.D (-) 100.00% 192

5000

96 ‘ I’’ 82 146 160 22.00 22.20 22.40 22.60

m/z-> 0 44 70। 118 11" ■' ।11" ।।"111"1 ■ i 11 ■ ।' i1' ।111111"11'1111' " I “ ■11 ■ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 IT. I.. k —l m/z 96.00 17.90% Abundance #103424: 3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192

5000 22.00 22.20 22.40 22.60 96 164 m/z 146.10 14.06% 138 0 11111011111111101111 —03-T‘‘"TITT TITTTT *—TT ’ITT m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192

22.00 22.20 22.40 22.60 5000 82 m/z 191.00 13.08% 54 110 0 30 -HP 11 " '' i " " i ■ " i " ■ ‘ i" I 16094 I '" i ‘"11"111" " i"111'1"111"11" if /z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102624:1,3-Benzodioxole, 4-methoxy-6-(2-propenyl)- (CAS)... 19/2 22.00 22.20 22.40 22.60 m/z 193.00 12.54%

5000

91 165 147| 103 119 131 177 । 0- ■ 1।।।"111""i"’ )"■ 11 ’ 11' " I ll. _I 111" 11 ’ I' ’■‘T " ‘ i ■ Hpt L m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

02086.D HP022102.M Wed Feb 27 08:35:02 2002 Page 13

NYC-WTC_000004621

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NYC-WTC_000004621Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999