DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000003981–000004147

Folder label: “GCMS X 1/29/02 A 2/1/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB01\30705.D Vial: 2 Acq On : 1 Feb 2002 3:34 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 3-Cyanocarbazole $$ 9H-Carb... Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

22.28 0.16 ug/L 119535 Phenanthrene-dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 72 2 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 3 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 58 4 6-Methoxy-2,4-dihydroxy-1,5-naph... 192 C9H8N203 000000-00-0 53 Abundance Scan 1656 (22.280 min): 30705.D (-) m/z 192.10 100.00% 192

5000 1 96 82 146 160 । 22.00 22.20 22.40 22.60

m/z-> 0 42 52 66 -mm 118 | , i i i | I I i ifl i'i i | i I I i | i i i I । I'l i . । , l4rTTUIIgu 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 1’8’3 m/z 96.10 17.43% Abundance #103424:3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192

5000 N 22.00 22.20 22.40 22.60 96 164 m/z 193.10 15.44% 138 n/z-> 0 ‘ ‘1’44’11*441/4111*1*111*1*11*11*4 m 1121’111111 1111 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588: 4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

22.00 22.20 22.40 22.60 108 5000 m/z 191.10 15.43%

146 175

0 !’1111’1111111710111—TT7TTTTII"T"T2-- i " " i1 ‘ " r '1' i " ■ l ■ 1 ■ ■ I ■ " H 1 1' i " " i Tp-I m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192 A 22.00 22.20 22.40 22.60 m/z 146.10 13.42%

5000 82

54 110

m/z—> 0 1 ■ "30I " '11 ‘ '11 ‘ " r " ‘ i " 111 94 -HP " । ■1 r i" " । 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 160 ।1" 11'" r ■' ■ i 41 4 ' ' i ' 1 ' ■ i ' ■ ' 1 i ' ‘ 22.00 22.20 22.40 22.60 ‘ i ■ ■'l “

30705.D SCAN508.M Mon Feb 04 08:41:32 2002 Page 12

NYC-WTC_000004105

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999