GCMS analysis report for sample AE01547, March 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB21\01547.D Vial: 3 Acq On : 21 Feb 2002 4:52 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 3-Cyanocarbazole $$ 9H-Carb... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

22.28 0.10 ug/L 68340 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 72 2 Phenanthrene , l-methyl- 192 C15H12 000832-69-9 59 3 Phenanthrene , 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 59 4 Phenant hrene, 2-methyl- 192 C15H12 002531-84-2 59 Abundance Scan 1675 (22.283 min): 01547.D (-) m/z 192.00 100.00% 192

5000

146 160 mz—> 0 60 70.42.4 70 ■ ■ i' ■ ■ • i1 ‘ • i ■ ■ ■ • i • ‘1 ■ i ■ ■

80 90 100 110 120 130 140 150 160 170 180 190 200 '111'1' i11111 — 22.00 22.20 22.40 22.60 m/z 193.00 16.26% Abundance #103424:3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192

5000 22.00 22.20 22.40 22.60 96 164 m/z 191.10 15.99% 138 0b । * I > > > > 11 >1 ■ I»r —*P*mPP I.... 1 ‘ I ‘‘ ' I' ‘ ‘ I TIE mfe-> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103924: Phenanthrene, 1-methyl- 192 T T TT 22.00 22.20 22.40 22.60 5000 m/z 146.00 15.34%

96 4EE 178 ob ....... ......... Il...... .......... ........... I ■. f 11 ■. .4 TITIr n/z—> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 11011 1512 22.00 22.20 22.40 22.60 m/z 96.10 12.06%

5000

96 165

miz—> 0b 60 70 80 88 1 90 139 100 110 120 130 140 150 160 170 180 190 200 152 । 176 4 22.00 22.20 22.40 22.60

01547.D. HP022102.M Mon Feb 25 10:55:26 2002 Page 13

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