GCMS analysis results for sample AE03075, March 5 2002

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Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.

NYC-WTC_000010887–000010906

Folder label: “GCMS X 2/5/02 A 2/28/02”

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NYC 9/11 Public Portal Document

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Data File : C:\MSDCHEM\1\5973N\02FEB28\02714.D Vial: 4 Acq On : 28 Feb 2002 1:00 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1. . .\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 3-Cyanocarbazole $$ 9H-Carb... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T.

22.28 0.11 ug/L 75734 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 64 2 1,3-Benzodioxole, 4-methoxy-6-(2... 192 C11H12O3 000607-91-0 64 3 l-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 4 (4ar,8ar)-4a,7,8,8a-tetrahydro-l... 192 C13H20O 107602-72-2 50 Abundance Scan 1675 (22.283 mln): 02714.D (-) m/z 192.00 100.00% 192

5000

96 82 146 160 22.00 22.20 22.40 22.60 01 anpil ■ i ■ ■ ■ ■ i • • ■ ■ i • ‘ ■ i ■ ■ • ■ i ■ ■1 ■ i ■ ■ ....... IIIIIII| 11— m/z 96.00 16.67% miz-> 80 90 100 110 120 130 160 170 180 190 200 140 150 Abundance #103424:3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192

5000 22.00 22.20 22.40 22.60 96 164 m/z 191.00 14.85% 138

mht~> 01 1101/2/0/21/0/8 -TPPPP 80 90 100 110 120 130 140 150 160 170 180 190 200 ■ ■ i ■ 1 i.... A Abundance #102624:1,3-Benzodioxole, 4-methoxy-6-(2-propenyl)- (CAS)... 192

22.00 22.20 22.40 2260 5000 m/z 146.10 14.62%

91 165 119 04 01 ■ i1 ■ ■ ■ । I ‘ 103 131 ,, , 147... 1 *I****I’ ’1***’I* —Pil-r-p-l 177

...... a.... n. । ■' • * । ■1 m/z-> 80 SO 100 110 120 130 140 150 160 170 180 190 200 Abundance #101918:1 -amino-2-methyl-4-isopropyl-thiotriazaphospholin... 159 192 22.00 22.20 22.40 22.60 m/z 193.10 13.84% 5000

144 177 , ... 0 ■ ■ i ■ ‘ ■ i • ■ ■ • i ■ ■ ■ ■ i ■ ■ ■ ■ i ■' ■ ■ । ‘ । ■ 1 1 i ' 1 1 1 1 1 ' ■ 1 i 1 ■' — /z-> 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

02714.D HP022102.M Fri Mar 01 10:07:02 2002 Page 13

NYC-WTC_000010903

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GCMS analysis results, sample AE02719, March 2002 · Box DEP Box 14

NYC-WTC_000010987

Gas chromatography-mass spectrometry analysis of sample AE02719 performed March 5, 2002, reporting other unknown compounds and surrogate 2,4-DDD recovery data.

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