GCMS analysis results for sample AE03075, March 5 2002

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Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB28\02714.D Vial: 4 Acq On : 28 Feb 2002 1:00 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1. . .\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

22.77 0.67 ug/L 454542 Phenanthrene- dl 0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 83 2 Phenanthrene-diO 188 C14D10 001517-22-2 64 3 N(l), N(2)-bis[(Furan-2-yl)methy... 188 C10H8N2O2 000000-00-0 45 4 Acridine-D9 188 C13D9N 000000-00-0 40 Abundance Scan 1718 (22.768 min): 02714.D (-) m/z 188.10 100.00% 188

5000

80 94 ।।.... 1 ■ P i i । i । । । i i । i

132 160 । 22.40 22.60 22.80 23.00

z-> 0- 30 40 +44.504+44 mmmH 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m/z 189.10 24.50% Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

) 5000- 22.40 22.60 22.80 23.00 1111 80 94 m/z 94.00 23.73% 158

mlz-> 0 i' 66 ■ i ■ ■1 ■ i" " i'1' ■ i ■ mmmmHTT 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 slam Abundance #84499: Phenanthrene-d10 188 . j .... 5 . Ttt| । j . 22.40 22.60 22.80 23.00 5000 m/z 80.05 19.61%

94 80 160 66 m/z—> 0-TPPmmmmpp — r....... lih.....W... 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #97589: N(1), N(2)-bis[(Furan-2-yl)methylene]hydrazine TIE 1 i 1 ■ 1 ■ i ■ 52 188 22.40 22.60 22.80 23.00 rn/z 184.00 12.08% 39 5000 80 94 103 131 66

miz-> 0 I‘ ’•I‘ ‘ • I —ala. | -n-p- Pmmmmpmnpmmmmm T’T 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 160 L mmm... .... I1 22.40 22.60 22.80 23.00

02714.D HP022102.M Fri Mar 01 10:07:02 2002 Page 14

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