DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000003981–000004147

Folder label: “GCMS X 1/29/02 A 2/1/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB01\31219.D Vial: 5 Acq On : 1 Feb 2002 6:03 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 22.77 0.44 ug/L 293683 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 64 2 3-Furanmethanol, 5-(phenylmethyl) - 188 C12H1202 000000-00-0 53 3 anti-10-hydroxy-5,6,8,9-tetrahyd... 188 C12H12O2 055139-53-2 50 4 2,2,9,9-Tetramethyldec-5-ene-3,7... 188 C14H20 102745-35-7 50 Abundance Scan 1699 (22.771 min): 31219.D (-) m/z 188.15 100.00% 188

5000-

94 66 80 160 22.40 22.60 22.80 23.00 23.20 44 52 m/z-> 0- " i"' IHmT ianbajbango TPTTTTTTHT 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 sell... m/z 94.00 16.50% Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 1$8

5000 22.40 22.60 22.80 23.00 23.20 80 94 m/z 184.10 10.64% 66 1 158 I I 0- ■ ■ । ■ ■ > > । •. ■ > (■ I' ।. mmmmmmmmmt ~nlz—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #98121: 3-Furanmethanol, 5-(phenylmethyl)- 188 ............ ........................................

22.40 22.60 22.80 23.00 23.20 5000 141 m/z 189.10 10.47% 129 104 157 I 170 0- ................. Il... 11111111'111111111'111111111111111' *11 " 1111 TT TPP n/z- > 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #98076: anti-10-hydroxy-5,6,8,9-tetrahydro-5,9-methano-7H-. 128 108 22.40 22.60 22.80 23.00 23.20 115 m/z 80-10 8.79%

5000 145

0 11—" i'' ■11 1’1 ■ i 1 ' 1 ■ i 1 ■ 1 1 i ■ /z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

31219.D SCAN508.M Mon Feb 04 08:41:50 2002 Page 14

NYC-WTC_000004048

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NYC-WTC_000004048Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999