DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000003981–000004147

Folder label: “GCMS X 1/29/02 A 2/1/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB01\31219.D Vial: 5 Acq On : 1 Feb 2002 6:03 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 Phenanthrene, 9-methyl- $$ ... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.13 ug/L 84534 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 59 2 2-CYANOCARBAZOLE $$ 9H-Carbazole... 192 C13H8N2 057955-18-7 50 3 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2 000000-00-0 49 4 1,3-Benzodioxole, 4-methoxy-6-(2... 192 C11H1203 000607-91-0 42 Abundance Scan 1656 (22.280 min): 31219. D (-) m/z 192.10 100.00% 192

5000

146 160 K.. 44 70 82 96 120 - 22.00 22.20 22.40 22.60 Of ----- ■ ■111 -■i-H • j1 r ■ TIPPPPPT 1’3 m/Z 146.10 17.86% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192

5000 A 1 22.00 22.20 22.40 22.60 m/z 191.10 16.32% 96 +l TTTpTt 4 165 88 II 139 152 176 0) 1' i111 b i' ' i ■11' i " " i ■ " 111111111111111111 " 1111 "'11111111111 Tl/Z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103420: 2-CYANOCARBAZOLE $$ 9H-Carbazole-2-carbonitrile (CAS 192

22.00 22.20 22.40 22.60 5000 m/z 193.10 16.18%

96 164 0 '' I ‘" 11 " 11' ‘' I " " I'' ‘' I' I rl11 " I " " 11" 11 "138 11'111" 1111111II111111" I' " 11 -rrp-i mlz—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102494: N-(2-methylprop-2-enyl)-2-nitrobenzenamine 192 22.00 22.20 22.40 22.60 77 151 m/z 96.10 13.35% 130 93 104 5000 119

177 0 11111111101111011000003 T’T’ -rj-i-r- TTT TTI3 ■ ।1 ■ ■ ■ ।" ■' । ■ ■ ■ ■ i ■ ■' ■ । I"' I" - m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

31219.D SCAN508.M Mon Feb 04 08:41:50 2002 Page 13

NYC-WTC_000004047

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NYC-WTC_000004047Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999