GCMS analysis results for sample AE00698, Jan 2002

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Laboratory report for sample AE00698 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050397–000050410

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN23\00698.D Vial: 6 . Acq On : 23 Jan 2002 7:05 pm Operator: Sample : 508 scan Inst : Inst rumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method . Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 Phenanthrene, 9-methyl- $$ ... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.

22.28 0.14 ug/L 83979 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 53 2 N-(2-methylprop-2-enyl)-2-nitrob. .. 192 C10H12N2O2 000000-00-0 49 3 l-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 45 4 1-Cyanocarbazole $$ 9H-Carbazole. .. 192 C13H8N2 083415-88-7 45 Abundance Scan 1656 (22.280 min): 00698.D (-) m/z 192.10 100.00% 192

5000 / X 96 146 160 22.00 22.20 22.40 22.60 44 70 82 0- n2mp -mmppmpmmmmmmmmpm m/z 193.10 15.40% miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 1512

5000 • ■ ■ i1 • > ■ if । ■ ■ ■ ■ । ■ 22.00 22.20 22.40 22.60 m/z 191.10 15.25%

miz-> 88 1 96 139 152 0- " i ■ •" i ■ •" I" 111'1111"11111'111' “ 11" 11" " 111 “'I'1" 11'1' 111111'1111'1111 Abundance 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 #102494: N-(2-methylprop-2-enyl)-2-nitrobenzenamine 165 ,| 176 , , u 192 77 151 130 22.00 22.20 2240 22.60 93 104 m/z 146.10 15.01% . 5000 119

177 0- ■ ■ i “ ■ ■ i ■ ■ ■ ■ t ■ ■ • • i ■' "i “ “ i T-rp- ’1’8 p-n- . 11.111111, ।।.... । L miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #101918:1 -amino-2-methyl-4-isopropyl-thiotriazaphospholin... ............ A P • ‘ I 1 ‘ ‘ • I ’ ’ ‘ 1 I ‘ 159 192 22.00 22.20 22.40 22.60 m/z 96.10 13.88% 5000

144 177 0 “I"I0I000115110m00*n—dm01m1g “ I * ‘ I'11 “ 1" rr " " I iz—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

00698.D SCAN508.M Thu Jan 24 09:57:23 2002 Page 6

NYC-WTC_000050406

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