GCMS analysis results for sample AE00101, Jan 2002

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Laboratory report for sample AE00101 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050370–000050383

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN23\00101.D Vial: 4 Acq On : 23 Jan 2002 5:25 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 1-amino-2-methyl-4-isopropy. .. Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.

22.28 0.14 ug/L 82393 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 l-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 2 N-(2-methylprop-2-enyl)-2-nitrob. .. 192 C10H12N2O2 000000-00-0 49 3 fluorene-9-spiro-cyclopropane 192 C15H12 000000-00-0 45 4 2-CYANOCARBAZOLE $$ 9H-Carbazole... 192 C13H8N2 057955-18-7 45 Abundance Scan 1656 (22,280 min): 00101.D (-) m/z 192.10 100.00% 1912

5000 . ... . ... pro 82 96 146 160 22.00 22.20 22.40 22.60

miz-> 42 66 0- —In—epTHg mmm 11 l1' 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 L m/z 191.10 14.82% Abundance #101918:1 -amino-2-methyl-4-isopropyl-thiotriazaphospholin... 159 1512

5000- .......n.... i\„ 22.00 22.20 22.40 22.60 144 177 m/z 96.00 13.88% |'i 1111 > ।. n 0- *1I!m’m—00"m01—"*m002—0003B Hp miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102494: N-(2-methylprop-2-enyl)-2-nitrobenzenamine 1912 77 151 130 22.00 22.20 22.40 22.60 93 104 m/z 193.10 12.57% 5000 119

177 0 ■ “ i “ “ i •' " i ■ “' i'' "i “ “ I TTIpr Tp-r ‘ “ 11 TIWWIPng 11 t'l 11 miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103959: fluorene-9-spiro-cyclopropane 1912 22.00 22.20 22.40 22.60 m/z82.10 10.78% 165 5000

87 $6 139 152 । t 0 mpsmmmoo 1 i. i 11 l iri j 1 17 11 i 1 | i i 1 | 131113 ................. / ' • i ■ ■ • ■ i 1 ■ ■ ' i 1 1 n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 2220 22.40 22.60

00101.D SCAN508.M Thu Jan 24 09:57:14 2002 Page 8

NYC-WTC_000050381

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