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GCMS analysis results for sample AE00101, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE00101 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050370–000050383

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\O2 JAN23\00101.D Vial: 4 Acq Ori : 23 Jan 2002 5:25 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 Phenanthrene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

22.77 0.27 ug/L 160767 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene-diO 188 C14D10 001517-22-2 86 2 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 83 3 Acridine-D9 188 C13D9N 000000-00-0 80 4 Acridine-D9 188 C13D9N 000000-00-0 72 Abundance Scan 1699 (22.771 min): 00101.D (-) m/z 188 .15 100.00% 188

5000 .. — ... 80 94 22.40 22.60 22.80 23.00 23.20 160 1 miz-> 0 -H 49 66 I --------------- 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m/z 189.10 17.22% Abundance #84499: Phenanthrene-d10 K6

—i |-i > i r-j i 1-1 t > -i < । i ■ i । । i 5000 22.40 22.60 22.80 23.00 23.20 80 160 m/z 80.10 16.20% 66 94 ----- 0 11' ■11 “ ■1111'11111 ■I.....I..... miz—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188 1 —rr . ‘ ' I ' ‘ ‘ I ‘ 22.40 22.60 22.80 23.00 23.20 5000 m/z 94.10 15.29%

80 94 66 158 , 1 0 11" 11" > ■ I' >111" 1' > I > I I mmmmmmmmmmmmmmmmmmmmm miz-> 40 50 60 70 80 90 1O> 110 120 130 140 150 160 170 180 190 Abundance #85254: Acridine-D9 ■ I 1 1 ‘ ‘ I ' ' ' Fi . . . i I . I 1 I I 1 1(8 22.40 22.60 22.80 23.00 23.20 m/z 184.10 10.01% 5000

158 93 66 80 I, niz—> 0-TmmTPmD 40 50 60 70 80 ..... .i.. 90 100 110 120 130 140 150 160 170 180 190 ....................... ......... 22.40 22.60 22.80 23.00 23.201

00101.D SCAN508.M Thu Jan 24 09:57:14 2002 Page 9

NYC-WTC_000050382

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NYC-WTC_000050382Source: NYC Law Department, mirrored locally

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