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GCMS analysis results, sample AE02718, March 2002

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Gas chromatography-mass spectrometry analysis of sample AE02718 performed March 5, 2002, documenting other unknown compounds and surrogate 2,4-DDD recovery at 97 percent.

NYC-WTC_000010967–000010986

Folder label: “GCMS X 2/5/02 A 2/28/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB28\02718 .D Vial: 3 Acq On : 28 Feb 2002 4:20 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 8, 2002 . Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 Phenanthrene-diO Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 22.77 0.44 ug/L 278511 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene-diO 188 C14D10 001517-22-2 86 2 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 86 3 Anthracene-dlO- 188 C14D10 001719-06-8 78 4 Acridine-D9 188 C13D9N 000000-00-0 50 Abundance Scan 1718 (22.768 min): 02718.D (-) m/z 188.10 100.00% 188

5000

49 66 80 92 132 158 . 22.40 22.60 22.80 23.00...... 0 i ■ ■ ■ '’i • ■ •11 ■ ■1 * 211 m/z 189.10 18.96% n/z-> 40 50 60 70 80 90 1(X) 110 120 130 140 150 160 170 180 190 Abundance #84499: Phenanthrene-d10 188

5000 22.40 22.60 22.80 23.00 ' ‘ ' 80 m/z 184.00 11.95% 94 160 66 miz-> 0- TmTTTT vaga 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 4419ll. Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d1 0 188 , L.... 22.40 22.60 22.80 23.00 m/z80.00 9.83% 5000

80 94 158 miz-> 66 0 BWEpmurtr orrt pmmm 40 50 60 70 80 90 1(X) 110 120 130 140 150 160 170 180 190 allamn Abundance #84502: Anthracene-d10- 188 22.40 22.60 22.80 23.00 m~r m/z92.00 9.70% 5000

66 80 94 160 , , - 0 I r‘'11111 ml i " ■ ■ —ii 111 • -P- I • ‘ > i • miz—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00

02718.D HP022102.M Fri Mar 01 10:07:29 2002 Page 14

NYC-WTC_000010984

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NYC-WTC_000010984Source: NYC Law Department, mirrored locally

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