GCMS DFTPP calibration report, Feb 5 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB05\28324A.D Vial: 3 Acq On : 5 Feb 2002 12:22 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 22.77 0.55 ug/L 611596 Phenanthrene-dl0 22.65

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 94 2 Phenanthrene-diO 188 C14D10 001517-22-2 87 3 Anthracene-diO- 188 C14D10 001719-06-8 83 4 Anthracene-D10 188 C14D10 000000-00-0 78 Abundance Scan 1699 (22.771 min): 28324A.D (-) m/z 188.20 100.00% 188

5000

80 94 66 132 146 158 22.40 22.60 22.80 23.00 23.20

/z-> 42 52 108 0- 111...... .. ■ । ■ H■i.■111■■11111 । . ................ ................. . 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 —149 TTm m/z 94.10 18.23% Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 22.40 22.60 22.80 23.00 23.20 80 94 m/z 80.05 16.26% 66 158 0- 1' I " ‘11 " 111 " 111■'1 ■ Tutt —TTTPm , I1 *|.|11. 1111" 11 miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84499: Phenanthrene-d1 0 188

22.40 22.60 22.80 23.00 23'20 5000 m/z 184.10 15.51%

80 94 160 66 - 0- ■' i ■ ' i ■'111 " ।11'1 n miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d1 0- ,... . 188 22.40 22.60 22.80 23.00 23.20 m/z 189.15 12.11%

5000

80 94 160 , .

tJz-> 0 TPTTPTP TTT 66

40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 l .... ............. 22.40 22.60 22.80 23.00 23.20

28324A.D SCAN508.M Fri Feb 22 11:44:13 2002 Page 13

NYC-WTC_000004874