GCMS DFTPP calibration report, Feb 5 2002

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Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\5973N\02FEB05\28324A.D Vial: 3 Acq On : 5 Feb 2002 12:22 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 Dibutyl phthalate $$ 1,2-Be... Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

24.85 0.03 ug/L 33738 Phenanthrene-dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Dibutyl phthalate $$ 1,2-Benzene... 278 C16H2204 000084-74-2 83 2 1,2-Benzenedicarboxylic acid, bu... 334 C20H30O4 000085-69-8 74 3 Dibutyl phthalate 278 C16H2204 000084-74-2 74 4 1,2-Benzenedicarboxylic acid, bu... 278 C16H2204 017851-53-5 64 Abundance Scan 1881 (24.849 min): 28324A.D (-) m/z 149.00 100.00% 149

5000 ................. ............................ 41 56 86 205 223 24.60 24.80 25.00 25.20 OA— li [ m/z 41.00 11.32% Tl/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #223242: Dibutyl phthalate $$ 1,2-Benzenedicarboxylic acid... 149 A

5000 24.60 24.80 25.00 25.20 m/z 150.00 10.25% 41 65 /6 104 121 205 223 278 0 ‘ I 1 1’ 41- i1 ■ i I’ । i । i11 । I' । i i |h । i i । i i" । । । i i i i । । t । 1i । । । . m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #284878:1,2-Benzenedicarboxylic acid, butyl 2-ethylhexyl ... 149 ..................... ............ , , , , , 24.60 24.80 25.00 25.20 5000 m/z 223.10 6.34%

76 56 104 121 । 160 205 223 278 n/z-> 0- Pp40—Hi 60 ' It 80 1 >'1 I l11 ■ i | 100 120 ‘ i ■ 1 140 160 । . . . . । . . . . । 180 200 । । । 'i . . 220 240 260 280 Abundance #223234: Dibutyl phthalate ■ ■ i ■ ■ 1 ■ । ‘ 1 i ■ ■ 149 24.60 24.80 25.00 25.20 m/z 85.90 5.97%

5000

57 76 104 121 205 223 250 278 0^ Mdtguddijuns l'"1 1 ‘ 1 1 1 "i i | । i । i | i । i । | r— . i .... i .... i . * ■ i ' TT-p-r /z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 24.60 24.80 25.00 25.20

28324A.D SCAN508.M Fri Feb 22 11:44:13 2002 Page 14

NYC-WTC_000004875

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