GCMS DFTPP calibration report, Feb 5 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB05\28324A.D Vial: 3 Acq On : 5 Feb 2002 12:22 pm Operator: Sample : 508 scan; re-ext Inst :Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 13 p-Terphenyl-dl4 Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 29.68 0.05 ug/L 51160 Chrysene-dl2 30.50 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 p-Terphenyl-dl4 244 C18D14 001718-51-0 50 2 9-Amino-l-phenyl-3,6-diazahomoad... 243 C15H21N3 000000-00-0 47 3 2-chloro-10-methyl-9-acridanone 243 C14H10C1NO> 000000-00-0 43 4 1,2-DICYANO-1,2-DIPHENYLCYCLOPRO. . . 244 C17H12N2 000000-00-0 42 Abundance Scan 2304 (29.678 min): 28324A.D (-) m/z 244.10 100.00% 244

5000 122 I \ A_______ ■p-r-r-r-J-r-n-r-p-r 86 108 170 198 212 29.40 29.60 29.80 30.00

n/z-> 43 O+ 1 I ’ ' 40 — 60 80 LL 100 120 140 160 I I I 180 200 220 240 I m/z 243.10 74.68% Abundance #160355: p-Terphenyl-d14 2414

5000 . K. 29.40 29.60 29.80 30.00 m/z 121.90 34.63% 122 01 ................... 196....... 160 184 198 212 226 „ m/z-> ■ i ■ ' 1 1 i 40 60 1 ' ' 1 i ■ ■ ' ■ i 1 ■ ’ ■ i ' 1 ' ■ i ■ 1 80 100 120 140 1 I ■ ■ ■ ■ i 1 ■ 160 TTT i il 180 200 220 240 Abundance #177798: 9-Amino-1 -phenyl-3,6-diazahomoadamantane 243 42 29.40 29.60 29.80 30.00 5000 56 m/z 245.10 32.47% 72 170 156 214 146 184 200 Of Tli I ■ ■ ' i ' ' ■ ' i ■ ■ ■ ■ i ' 1 ' ' i 1 ' n/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #177573:2-chloro-10-methyl-9-acridanone ....... ...... .. 243 29.40 29.60 29.80 30.00 m/z 242.10 18.16%

5000

co 75 ,no — . 200 214 228 0 ............ ...... 198..... 150, ,, 174, . L ,, k . I ,.... n/z—> 40 60 80 100 120 140 160 180 200 220 240 29.40 29.60 29.80 30.00

28324A.D SCAN508.M Fri Feb 22 11:44:13 2002 Page 15

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