GCMS analysis results for sample AE00842, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB07\00842.D Vial: 6 Acq On : 7 Feb 2002 6:34 pm Operator: . Sample : 508 scan Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 12 p-Terphenyl-dl4 Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

27.54 0.11 ug/L 67550 Chrysene-dl2 30.49

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l p-Terphenyl-dl4 244 C18D14 001718-51-0 91 2 5-HYDROXY-5,6-DIDEHYDROKAWAIN $$... 244 C14H1204 060037-36-7 58 3 2-Benzylbiphenyl 244 C19H16 000000-00-0 42 4 2-Methylene-2b-methyl-3,3-dimeth... 244 C14H16N2O2 000000-00-0 37 Abundance Scan 2117 (27.543 min): 00842.D (-) m/z 244.20 100.00% 2.14

5000

122 11 49 80 94 106 I 160 212 > i 27.20 27.40 27.60 27.80 0 1 ------ 1 1 — ................................................................ ...............i|il[l m/z 122.10 17.43% m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #160355: p-Terphenyl-d14 2-4

5000 AA ‘ 'I 27.20 27.40 27.60 27.80 11

m/z 243.20 17.02% . 122 0T 196, . 10111184 198, j" 276, ui /z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #178835: 5-HYDROXY-5,6-DIDEHYDROKAWAIN $$ 2H-Pyran-2-one, ... 131 244 69 103 TTF 27.20 27.40 27.60 27.80 5000 84 m/z 245.20 13.24%

145156 13183 199 — 0i ■ ■ ■ ■ i ■ ■ ■ ■ i n/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #179624:2-Benzylbiphenyl T T I-1 2.14 27.20 27.40 27.60 27.80 m/z 240.10 11.03% 165 5000 229

l 152 ............... -> 0 60 80 100 120 140 11 160 180 200 220 240 27.20 27.40 27.60 27.80

00842 .D HP020702.M Thu Feb 21 09:58:10 2002 Page 14

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