GCMS analysis results for sample AE00842, Feb 2002

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Laboratory report showing GCMS analysis of sample AE00842 including surrogate recovery and unknown compounds.

NYC-WTC_000052251–000052270

Folder label: “GCMS X 1/11/02 A 2/7/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\5973N\02FEB07\00842 .D Vial: 6 Acq On : 7 Feb 2002 6:34 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 13 Bis(2-ethylhexyl) phthalate Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

31.11 0.19 ug/L 118534 Chrysene-dl2 30.49

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Bis(2-ethylhexyl) phthalate 390 C24H3804 000117-81-7 72 2 1,2-Benzenedicarboxylic acid, bi... 390 C24H3804 000117-81-7 72 3 Bis(2-ethylhexyl) phthalate 390 C24H3804 000117-81-7 64 4 1,2-Benzenedicarboxylic acid, di... 390 C24H3804 027554-26-3 64 Abundance Scan 2429 (31.105 min): 00842.D (-) m/z 149.00 100.00% 149

5000 167 226 AA.............. . , ...................... J 84 113 207 279

m/z-> 01 LL --- 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 mm 30.80 31.00 31.20 31.40 m/z 167.00 38.06% Abundance #326909: Bis(2-ethylhexyl) phthalate 149

5000 57 167 30.80 31.00 31.20 31.40 m/z 57.10 26.74% 279

m/z-> 0 83.1 ,1113,4132/ TT । 1 ।■■■ • । • ■ • ■ । ■' ■■।■•■• ।" 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 i ■ " ' r ''' i1 ‘ ■ r '' ’ 1

Abundance #326902:1,2-Benzenedicarboxylic acid, bis(2-ethylhexyl) e... 149 TTT 30.80 31.00 31.20 31.40 A J Tll

5000 57 m/z 71.10 24.92% 167 83 113 279 0- " i" J| i il I |l|L i i i । ।I | J |‘i132 IH|J . .......... 1....... ??0 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #326913: Bis(2-ethylhexyl) phthalate 149 30.80 31.00 31.20 31.40 m/z 43.10 24.27%

5000 167 57 279

m/z-> 0 II|III 183 113 11 A I | !| I I f 111 |l 11 TTTT r ■'' r ■ ■' i " " i r '" i' " ' r " ■ r ' " i 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 1 1 30.80 31.00 31.20 31.40

00842.D HP020702.M Thu Feb 21 09:58:10 2002 Page 15

NYC-WTC_000052269

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