GCMS analysis results for sample AE03248, March 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03248 conducted on March 15, 2002.

NYC-WTC_000006146–000006165

Folder label: “GCMS X 2/12/02 A 3/01/02”

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NYC 9/11 Public Portal Document

Data File: C:\MSDCHEM\1\5973N\02MAR01\03248.D Vial: 3 ' Acq On : 1 Mar 2002 5:39 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 (IS*,2R*,5R*,7S*)-2,4-Dimet... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 31.09 0.08 ug/L 49941 Chrysene-dl2 30.49 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 (IS*,2R*,5R*,7S*)-2,4-Dimethyl-7... 168 C10H16O2 091926-28-2 72 2 1,2-Benzenedicarboxylic acid, 3-... 211 C8H5NO6 000603-11-2 56 3 Phthalic acid, diisooctyl ester ... 390 C24H3804 001330-91-2 56 4 1,2-Benzenedicarboxylic acid, di... 390 C24H3804 027554-26-3 56 Abundance Scan 2455 (31.088 min): 03248.D (-) m/z 149.00 100.00% 149

5000- 167 57 71

m/z-> 0—

Abundance 40 41

1 I ■ 60 80 83

■ ■ ' I ' 100 + 97 113

120 140 I*IIIIIIII**II/ 160 | 180 200 220 #70509: (1 S*,2R*,5R*,7S*)-2,4-Dimethyl-7-ethyl-6,8-dioxabi... 207 240 240 30.80 31.00 31.20 31.40 m/z 167.00 ‘ 14* ‘ I‘*

40.13%

149

5000 167 30.80 31.00 31.20 31.40 57 m/z 71.00 29.00% 83 113 ..... I 0-' 1 i ' 1 ' 1 i ' 1 1 1 I ' 1 1 I 1 1 । ' I 1 1 11 1 1 1, ' I ' IP miz-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #131213:1,2-Benzenedicarboxylic acid, 3-nitro- (CAS) $$ 3... 149 N ■ ' l 1 ' 30.80 31.00 31.20 31.40 1 i 1 1

m/z 57.05 26.37%

M 5000 167 71

n/z-> 0- —40 60 4 83 i 113 132 1 i । h > ■ ■ i 1 . 11. i"i ' i । । । 1 . । . 11 I I I III I I I I I I80 100 120 140 160 180 200 220 240 Abundance #326955: Phthalic acid, diisooctyl ester $$ 1,2-Benzenedic... 149 30.80 31.00 31.20 31.40 m/z 70.10 22.54%

5000 57 167 71 83 — 113 ,

m/z-> 0 ..... 40 as"60 T l 1 । i । । i । i i । । । । । । । । । । । । 1 ■ < । 1 1 1 ■ i ' ■ ■ 1 । 1 ■ ■ 1 । 1 ■ 80 100 120 140 160 180 200 220 240 ■ ■ I ■ ■ ■ ■ I ■ ' p ' 1 1 I 1 1 30.80 31.00 31.20 31.40

33248.D HP022102.M Mon Mar 04 12:33:29 2002 Page 15

NYC-WTC_000006164

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GCMS analysis results for sample AE03245, March 2002 · Box DEP Box 12

NYC-WTC_000006085

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03245 conducted on March 15, 2002.

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