GCMS analysis results for sample AE03075, March 5 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

■ * Data File : C:\MSDCHEM\l\5973N\02FEB28\02717.D Vial: 2 Acq On : 28 Feb 2002 3:30 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 Phthalic acid, diisooctyl e... Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

31.10 0.04 ug/L 23756 Chrysene-dl2 30.49

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phthalic acid, diisooctyl ester ... 390 C24H3804 001330-91-2 72 2 1,2-Benzenedicarboxylic acid, bi... 390 C24H3804 000117-81-7 72 3 1,2-Benzenedicarboxylic acid, di... 390 C24H3804 027554-26-3 72 4 (1S*,2R*,5R*,7S*)-2,4-Dimethyl-7... 168C10H16O2 091926-28-2 64 Abundance Scan 2456 (31.099 min): 02717.D (-) m/z 149.00 100.00% 149

5000

41 57 70 113 167 207 239 ...... 0....... 30.80 31.00 31.20 31.40 0Amor ■ ‘ 1 ■ ■ ■ • i ■ ‘ ' i ‘ ‘ ‘ ‘ 1 ‘ ■ ' 1 1 ' ■ ' i ■ ■ • ■ i ‘ ‘ i ‘ ■ 1 I ■ ‘ ■ i ■ • m/z 167.00 33.37% miz-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #326955: Phthalic acid, diisooctyl ester $$ 1,2-Benzenedic... 149

5000- 1 ■ i 1 • ■ • i ■ ‘1 1 1 1 ' I 1 1 57 167 30.80 31.00 31.20 31.40 71 m/z 57.10 28.02% 18 97 0- - ■ 1 ■ 1 ■ 1 1 ' * 113 1 1 1 I 1■ ■ i ■ ■ ■ • i ■ ■ ■ ■ i ■ '

miz-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #326907:1,2-Benzenedicarboxylic acid, bis(2-ethylhexy!) e... 149 1 ■ i ■ ■ ■ ■ i • ' 1 1 ' 1 11 I ' 1 30.80 31.00 31.20 31.40 5000 m/z 55.10 20.68% 57 167 71 83 — 113 , O — l .97 42 • ‘ I 1 ..Il ,,, —————————— 1 I'T 1 171 । r i r 1 । 1 1 1 1 । 1 . 1 1 j 1 miz-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #326921:1,2-Benzenedicarboxylic acid, diisooctyl ester (C... 149 30.80 31.00 31.20 31.40 m/z 70.00 19.51% 5000 57 167 71

m/z—> 0- ' i 1 '' 40 48. 60 80 100 113 ■ i ■ ■ ■ • i ■ • ■ • l ■ 1 ■ ■ i ■ ■ ■ 1 1 ' • ■ ■ । 120 140 160 180 200 220 ■ 1 ■ *

240 141" Pri i ' 1 i ' ' 1 1 l‘ ' 30.80 31.00 31.20 31.40

02717.D HP022102.M Fri Mar 01 10:07:23 2002 Page 15

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