GCMS analysis results for sample AE03248, March 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03248 conducted on March 15, 2002.

NYC-WTC_000006146–000006165

Folder label: “GCMS X 2/12/02 A 3/01/02”

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NYC 9/11 Public Portal Document LDrary searen compound Report

Data File : C:\MSDCHEM\1\5973N\02MAR01\03248.D Vial: 3 ' Acq On : 1 Mar 2002 5:39 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 N-perdeuteriobenzylideneani... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

22.28 0.13 ug/L 90534 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 58 2 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 53 3 Benzo[l,2-c:3,4-c]bis(isothiazol... 192 C8H4N2S2 074960-05-7 53 4 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2 000000-00-0 46 Abundance Scan 1675 (22.283 min): 03248.D (-) m/z 192.00 100.00% 19/2

5000

96 42 70 82 146 160 22.00 22.20 22.40 22.60 0 1 r11' i11111" " i1 ''11 r'111'"1 r?ri 111'" I ■11111111111! ।" 11111111111 TPT m/Z 191.00 19.40% /z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192

5000 82 22.00 22.20 22.40 22.60 54 m/z 96.00 17.15%

m/z—> Abundance 0 " "30 94 11" ‘ r 11 ■ r > ■ ।"111 ■ । ■ i ■ ■Hl.. 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 110 160 TTIUOTTUTTTTTTTIWWTTTTTWTTTTTTT+

#102098: Thiocyanic acid, 2-benzothiazolyl ester (CAS) $$ ... u 192

22.00 22.20 22.40 22.60 5000 m/z 193.10 15.11%

,8290 1 I8 122 134 148 160 /z—> 0 " I " " I " ‘ ' I ' 1 " I " " I " ' 1 P " T"" ' ' I 1 rT I I I I I | I ! I I | I I I I | I I I I | I I ! I | I !'I I | I ! I I | I M | | 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 4— Abundance #102104: Benzo[1,2-c:3,4-c]bis(isothiazole) $$ Benzo[1,2-c... 192 22.00 22.20 22.40 22.60 m/z 146.10 15.04%

5000 45 148 57 69 82 96 121 .......................... ............ ........ 0 ... ,,,,.. I.. I.. i.. |..... 1.... ..... .............. l|.... " i " '111 ■111 * ’ * * i ■ ■1 ■ i1 ■ " i1" TT‘ ■1 ■ r 1" i " ■1 |IT 1111' । ] 11 ' I " " I ' '' 1 I ' 1 1 1 I " 1 ' 1’1 1 I " mfe—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

3248.D HP022102.M Mon Mar 04 12:33:29 2002 Page 14

NYC-WTC_000006163

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GCMS analysis results for sample AE03245, March 2002 · Box DEP Box 12

NYC-WTC_000006085

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03245 conducted on March 15, 2002.

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