GCMS analysis results for sample AE00844, Feb 26 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB07\00844.D Vial: 7 Acq On : 7 Feb 2002 7:24 pm Operator: . Sample : 508 scan Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l..-\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 1,2-Benzenedicarboxylic aci... Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

31.11 0.06 ug/L 36595 Chrysene-dl2 30.49

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Benzenedicarboxylic acid, di... 390 C24H3804 000117-84-0 43 2 1,2-Benzenedicarboxylic acid, di... 390 C24H38O4 027554-26-3 43 3 (IS*,2R*,5R*,7S*)-2,4-Dimethyl-7... 168 C10H16O2 091926-28-2 42 4 1,2-Benzenedicarboxylic acid, bi... 390 C24H38O4 000117-81-7 33 Abundance Scan 2429 (31.105 min): 00844.D (-) m/z 149.10 100.00% 149

5000 167 57 84 113 207 226 ALA4 30.80 31.00 31.20 31.40 TTI

o1 TT000011117 rp-rrn > , | i . > p ‘T 11" " FT" 1 ■ i " ■ ■ i " '11'1" i i' ■ " i" 11 r 11' i m/z 167.00 42.06% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #326898:1,2-Benzenedicarboxylic acid, dioctyl ester (CAS)... 149

J > l < 1 । • l ■ ■■ ■ < I 5000 57 167 30.80 31.00 31.20 31.40 m/z 57.10 28.34% 390 0 TTTTT TI—p—u0—‘u*m—nT‘T r"'i""i m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #326922:1,2-Benzenedicarboxylic acid, diisooctyl ester (C... 149 ■ ■ i ■ ■ • ■ i ■ i ■ ' ' k i ' TTI 30.80 31.00 31.20 31.40 5000 m/z 113.10 24.85% 57 167

390 0 ' ‘ i " 111' " ' i" ■' r " ' i '11'' " I I' " ' I ’'' ’ I'" ’ I " " I " " I I ■'' ■ I l ‘1 n I n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #70509: (1 S*,2R*,5R*,7S*)-2,4-Dimethyl-7-ethyl-6,8-dioxabi... 149 +T 30.80 31.00 31.20 31.40 m/ z 43.10 23.52% M 5000 167

71 113

m/z-> 0 — L " I' 111 }'1'11" " I ‘'1' 11 ’'' I " ’ ’’I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 i1 ■" i ’"' i" " i" " i 1 ' 1 1 1 ' ' 1 1 1 1 I ' 1 '• । ."< > । । 30.80 31.00 31.20 31.40

00844.D HP020702.M Thu Feb 21 09:58:18 2002 Page 14

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