GCMS analysis results for sample AE00844, Feb 26 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB07\00844.D Vial: 7 Acq On : 7 Feb 2002 7:24 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ****************************************************************** * * * Peak Number 13 Tetrapentacontane Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T.

34.94 0.06 ug/L 28367 Perylene-dl2 34.42

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Tetrapentacontane 759 C54H110 005856-66-6 47 2 2-t-Butyl-3-ethoxycarbonyl-5,5-d... 241 C13H23NO3 062020-96-6 43 3 1-Heptanol, 2-propyl- $$ 2-Propy... 158 C10H22O 010042-59-8 38 4 4-Octanone 128 C8H16O 000589-63-9 37 Abundance Scan 2765 (34.941 min): 00844.D (-) m/z 57.10 100.00% 57

5000 96 265 " I 1 r1 1 r1 1I 1 1 1 1 I' ' 1 1 1 1 34.60 34.80 35.00 35.20 01 T 1111111111111111' i1111111 ■11 ■1 ■b ।111' i11 ’ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■' ■ ■ i11 ■ ■ । m/z 71.10 96.42% miz-> Abundance 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 57 #389371: Tetrapentacontane 1 5000 TT — 34.60 34.80 35.00 35.20 m/z 43.10 90.25% 379 421 575 617 659 701 758 o1 1uu‘uuuTumu‘n—uu‘0‘u—""—Trr m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 Abundance #175049: 2-t-Butyl-3-ethoxycarbonyl-5,5-dimethyl-1 -pyrroli... 57 । । ' 1 । ' । । ' 1 1 11 1 1 1 1 34.60 34.80 35.00 35.20 5000 m/ z 85.10 71.89% 99 136 241 0- ■ । ‘1 1—00—000—0000—001—000000011000001101111 i1 •' ■ i11 ■ ‘ i miz-> 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 Abundance #58290:1 -Heptanol, 2-propyl- $$ 2-Propylheptanol TCEunmm I ' 1 """I 1 1 1 1 43 34.60 34.80 35.00 35.20 m/z 96.00 35.92%

5000 85

| 126 o TTTT "II.I.................... . . . . . ।1।.. . .......... ....................... .................... ■ 1 I ’ 1 1 ■ II ItT TTtr TIl /z-> 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 34.60 34.80 35.00 35.20

00844.D HP020702.M Thu Feb 21 09:58:18 2002 Page 15

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