Quality control report for GCMS analysis of sample AE00277 showing surrogate recovery data from January 10, 2002.
NYC-WTC_000050838–000050855Folder label: “GCMS X 1/7/02 A 1/9/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File : C:\MSDCHEM\l\5973N\02JAN09\277.D Vial: 2 Acq On 9 Jan 2002 6:59 pm Operator: - Sample : 508 scan ext 1/7 Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 4-Heptanone, 2,6-dimethyl- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.
8.85 0.22 ug/L 97358 1,4-Dichlorobenzene-d4 9.72
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 4-Heptanone, 2,6-dimethyl- 142 C9H180 000108-83-8 86 2 4-Heptanone, 2,6-dimethyl- $$ s-... 142 C9H180 000108-83-8 86 3 4-Heptanone, 2,6-dimethyl- (CAS)... 142 C9H180 000108-83-8 86 4 4-Heptanone, 2,6-dimethyl- (CAS)... 142 C9H180 000108-83-8 86 Abundance Scan 480 (8.854 min): 277.D (-) m/z 57.10 100.00% 57 85
5000 41
69 97 127 142 ■ ' i ■ f ■ 8.60 A 8.80 9.00 9.20 01 ' ' I 1 1 " I 1 ' ' ' T -74 ■'i ‘ ■ i ''1 ■ i • I m/ z 85.10 85.62% ‘I 1 11 1 TT m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #38602: 4-Heptanone, 2,6-dimethyl- 57 85
5000 41 8.60 8.80 9.00 9.20 m/z 41.10 30.76% 27 142 69 127 OPTT ,..■1....... Il....... IT 1 I ' ' I • I ' 100 H TWWIIPT - m/z-> 10 20 30 40 50 60 7080 90 100 110 120 130 140 150 Abundance #38600: 4-Heptanone, 2,6-dimethyl- $$ s-Diisopropylacetone... 57 85 I—MM— ... ....... ft 8.60 8.80 9.00 9.20 5000 m/z 58.00 26.50% 43 27
15 J 0- TTt‘‘‘11 TTTT PPP, rra 69 --- - 100 .... 127. 142 TTT m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #38606:4-Heptanone, 2,6-dimethyl- (CAS) $$ 2,6-Dimethyl-4... 57 8.60 8.80 9.00 9.20 85 m/ z 43.10 22.50%
n/z-> 5000
0 m 10 20 27
30 41
40 50 60 69 TIT I’i1 ■ ■ 'i' 70 ■ i ■ ■1 • i ■
80 90 100 1 I ' * ' ' I 127 100 110 120 130 140 150 142 — A. y 8.60 8.80 A *TT 9.00 9.20
277.D SCAN508.M Thu Jan 10 11:51:37 2002 Page 9
NYC-WTC_000050851
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000050893
Laboratory record documenting GCMS surrogate recovery data for sample AE00280 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050912
Laboratory record documenting GCMS surrogate recovery data for sample AE00281 analyzed on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050875
Laboratory record documenting GCMS surrogate recovery data for sample AE00279 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050932
Laboratory record documenting GCMS surrogate recovery data for sample AE00282 analyzed on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051755
GCMS analysis log for sample AE00561 showing surrogate recovery and unknown compounds detected on January 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050856
Laboratory record documenting GCMS surrogate recovery data for sample AE00278 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050963
Laboratory record documenting GCMS surrogate recovery data for sample AE00316 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050977
Laboratory record documenting GCMS surrogate recovery data for sample AE00317 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051727
Laboratory report showing GCMS analysis results for sample AE00559 conducted on January 17, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051685
Laboratory report showing GCMS analysis results for sample AE00365 conducted on January 17, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051586
Laboratory report showing GCMS analysis results for sample AE00613 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050948
Laboratory record documenting GCMS surrogate recovery data for sample AE00310 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000050813
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050814
Fragmented page from a DEP laboratory record showing method parameters and sample data fields for January 7-9, 2002 testing.
Filed in the same folder
NYC-WTC_000050817
Technical form detailing GCMS analysis results for sample AE00277 listing detected compounds and concentrations from January 9-10, 2002.
Filed in the same folder
NYC-WTC_000050821
Reference report for GCMS analysis of sample AE00277 listing compound names and qualifier values from January 9-10, 2002.
Filed in the same folder
NYC-WTC_000050825
Blank analysis report for GCMS of sample AE00277 showing compounds below method detection limits from January 10, 2002.
Filed in the same folder