GCMS surrogate recovery results for sample AE00280, Jan 2002

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Laboratory record documenting GCMS surrogate recovery data for sample AE00280 analyzed on January 10, 2002.

NYC-WTC_000050893–000050911

Folder label: “GCMS X 1/7/02 A 1/9/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN09\280.D Vial: 5 Acq On 9 Jan 2002 9:31 pm Operator: Sample : 508 scan ext 1/7 Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 6 3-[.beta.-hydroxy-(.beta.,.. Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T. 5.70 0.16 ug/L 79685 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-[.beta.-hydroxy-(.beta.,.beta... 86 C5H6D20 005557-87-9 50 2 l-Heptene, 4-methyl- $$ 4-Methyl... 112 C8H16 013151-05-8 39 3 Pentane, 2-methyl- (CAS) $$ 2-Me... 86 C6H14 000107-83-5 38 4 CIS-1-METHOXY-2-BUTENE 86 C5H10O 010034-14-7 37 Abundance Scan 204 (5.703 min): 280.D (-) m/z 41.10 100.00% 41 71

5000

........................ ................... 53 58 84 5.40 5.60 5.80 6.00

m/z-> 0+ I" " I ml 4, ■... MHi........Li...... 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 i*■ "r"•i T‘ m/z 43.10 .99.26% Abundance #3392:3-[.beta.-hydroxy-(.beta.,.beta.-clideuterio))ethylp... 71

5000 — ————————— 58 85 5.40 5.60 5.80 6.00 53 m/z 71.10 75.63% 44 ।■••■।•i■ ” ■i■।•11 ■ ■ • • । fill l"l""l"'l l'i'i■"'।

L 0 T’’ i ■■ "i" " r " 'i" " r n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 Abundance #13981:1 -Heptene, 4-methyl- $$ 4-Methyl-1 -heptene 43 ... 70 T"I 5.40 5.60 5.80 6.00 5000 55 m/z 39.10 59.11%

27 0 a v HT "IFT T 84 r "' r "'r " T"' r1 "i ■■ ■■ । ■ 112 m/z-> Abundance 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 #4261: Pentane, 2-methyl- (CAS) $$ 2-Methylpentane $$ Isoh... 43 —.... No. 5.40 5.60 5.80 TIM 6.00 m/Z 69.10 52.05% 5000 71 57 m/z-> 0 l • i«" < i < < •1 ] 11 > 111' ।।| + 86 i • > • ■ 11 ■ ■ ■ । 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 i’■" i■•i • ’• ■ i ’1'11 i• 5.40 5.60 5.80 6.00 ‘ I

280.D SCAN508.M Thu Jan 10 11:51:55 2002 Page 8

NYC-WTC_000050905

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