GCMS analysis results for sample AE03250, March 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03250 conducted on March 15, 2002.

NYC-WTC_000006186–000006205

Folder label: “GCMS X 2/12/02 A 3/01/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02MAR01\03250.D Vial: 5 , Acq On : 1 Mar 2002 7:18 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 3-Penten-2-ol (CAS) $$ 2-PE... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 5.71 0.10 ug/L 47913 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Penten-2-ol (CAS) $$ 2-PENTEN-... 86 C5H10O 001569-50-2 53 2 2-Furanmethanol, tetrahydro- (CA... 102 C5H10O2 000097-99-4 50 3 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 50 4 4-Penten-2-ol (CAS) $$ PENT-4-EN... 86 C5H10O 000625-31-0 40 Abundance Scan 207 (5.711 min): 03250.D (-) m/ z 41.10 100.00% 41 71

5000 45 84 --------- 53 58 5.40 5.60 5.80 6.00 m/z-> 5 Or II’ 11"' ■ i ■ ■ ■ ■ i ■ " 11" " । " 111 49 4 - — 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 11 ■1 " i m/z 43.10 88.21% Abundance #4043:3-Penten-2-ol (CAS) $$ 2-PENTEN-4-OL $$ Methyl prop... 43 71

5000 27 —mmmTERTTT 5.40 5.60 5.80 6.00 15 53 m/z 71.10 84.73% 31 58 67 86 0b 111 ■' 35.... I " 11" " r 11 r*"11" " i'1 TT - 11 ‘ ।111 ।111" 111111' I''1' i " " i miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #9384: 2-Furanmethanol, tetrahydro- (CAS) $$ Tetrahydrofur... 7h 43 ............ ................................. -■ 1■ i ■ ■1 1 i ■ ■ ‘ ■i1111 111 5.40 5.60 5.80 6.00 5000- 27 m/z 69.10 52.95% 31

Of 37 "If ........ "I' " i " " i " ‘' i " 1' i ■ 1.... . ......... ।■ i " " i' " 11" ‘' i " " i n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #4085: 3-Buten-2-ol, 2-methyl- ........ A...................... ■ 1 । ■ 1 1 1 । ■ 1 1 । 1 > > r ।

43 71 5.40 5.60 5.80 6.00 m/ z 45.00 30.86%

5000 59 27 31 53 671 86 oh '' i " " i " 111 ■ " ' r TTI " i " " i'' HH 1" " 11 11 —1TTTPTTPTTTT IIIIIII- TTIm m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 5.40 5.60 5,80 6.00

33250.D HP022102.M Mon Mar 04 12:33:41 2002 Page 10

NYC-WTC_000006199

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