GCMS analysis results for sample AE00169, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE00169 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.

NYC-WTC_000050519–000050538

Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02”

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NYC 9/11 Public Portal Document **.Z

Data. File : C: \MSDCHEM\1\5973N\02JAN24\00169 .D Vial: 2 . Acq On : 24 Jan 2002 3:48 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1. . .\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 3-Buten-2-ol, 2-methyl- (CA... Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 5.02 0.14 ug/L 71387 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Buten-2-ol, 2-methyl- (CAS) $$... 86 C5H10O 000115-18-4 78 2 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 50 3 Butenol, methyl- 86 C5H10O 060766-00-9 50 4 2-Furanmethanol, tetrahydro- (CA... 102 C5H10O2 000097-99-4 47 Abundance Scan 144 (5.018 min): 00169. D (-) m/z 71.10 100.00% 43 71

5000

39 51 i 55 59 67 85 AA 4.60 4.80 1 ■ i 1 ■ • ■ i ■ ■ ■ ■ i ■ ■ 5.00 5.20 5.40

nz-> ll'lll.. 11... mHmmm ‘1 “i‘• ”i■ ■ “ ii“‘11“"11 “ +44 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 । ■ 1111 m/z 43.10 90.57% Abundance #4088:3-Buten-2-ol, 2-methyl- (CAS) $$ 2-Methyl-3-buten-2... 7h

5000 NA N A Wy4o A N 59 4.60 4.80 5.00 5.20 5.40 m/z 41.10 51.84% TPHH 67, 1u1 , 85

N l ""I"“I ।‘ ।■11 ■ •1 ■ । । —00’0—BETTT nfe-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #4084:3-Buten-2-ol, 2-methyl- 71 43 N A , A Al 4.60 4.80 5.00 5.20 5.40 5000 m/z 69.10 30.64% 59

27 53 67 86 mmmmmmmmmmmm ‘I-mHH hn ,.ii. ।. i.. 111. :,11 . i । m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #4093: Butenol, methyl- ■ ■ i ■ ■ ■ ■ i ■ ' 43 71 4.60 4.80 5.00 5.20 5.40 m/z 59.10 29.35%

5000 59 27

JU 15 31 53 “ " i ■ ■ ■ ■ TTT-p-rrrp- ' ‘ l ' ' ‘ I ‘ ‘ I' ' 67 , aal—l TTHH 86 1" i■ ■1' i‘ ■ ■ ■ i" “ i"'11 A........ / 1 i 1 • • ■ i ■ ‘ ■nfz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 4.60 4.80 5.00 5.20 5.40

>0169.D SCAN508.M Fri Jan 25 10:25:59 2002 Page 7

NYC-WTC_000050529

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NYC-WTC_000050481

Laboratory report for sample AE00167 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.

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